Synthesis of New Oxidant N-chloroisonipecotamide and its Oxidation Kinetics on Aromatic Acetals

Shenbagam, K.; Mathiyalagan, N.

doi:10.13005/ojc/290253

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“…Recrystallization of NCP was done with ether solvent. 15 Fig. -1: Rection for the preparation of N-Chloropicolinamide…”

Section: Methodsmentioning

confidence: 99%

Synthesis and Characterization of N-Chloropicolinamide: A New, Mild, Stable, Effective and Efficient Oxidant for Organic Substrates

Subalakshmi¹,

Priya²

2019

RJC

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The new oxidant N-Chloropicolinamide (NCP) is synthesized by the chlorination of picolinamide using trichloroisocyanuric acid. The physical constant, formal redox potential, element analysis and spectra characterization (IR, UV, 1 H-NMR, C 13 -NMR and mass spectrum) confirms the presence of nitrogen-halogen bond. It is prepared by a simple method giving a high yield in a short period of time. It is found to be a mild and stable oxidant and formal redox potential of N-chloropicolinamide shows that it can be used as an effective source of positive halogen.

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“…Recrystallization of NCP was done with ether solvent. 15 Fig. -1: Rection for the preparation of N-Chloropicolinamide…”

Section: Methodsmentioning

confidence: 99%