“…7a and b, respectively, is probably due to the combustion of decomposed residual ethanol. 46 Because no weight loss is detected, the exothermic peaks at 963 • C in Fig. 7a and 935 • C in Fig.…”
“…7a and b, respectively, is probably due to the combustion of decomposed residual ethanol. 46 Because no weight loss is detected, the exothermic peaks at 963 • C in Fig. 7a and 935 • C in Fig.…”
“…processes, YAG:Ce can be prepared by sol-gel [1,10], glycothermal [8], precipitation [11,12], and polymer [13]. From these processes, typically amorphous particles were produced in the first step of preparation.…”
“…According to this, the calcining temperature should be above 1029.5 • C. In this paper, a calcining temperature of 1050 • C was chosen to obtain the nanopowders with a pure YAG phase and high sintering activity. The Nd:YAG precursors are carbonate and hydroxide mixed precipitates, and the partial Al hydroxide dissolved as Al(OH) 4− ions at pH value above its isoelectric point range of ∼8.5-9.5 in the slurries, while the isoelectric points of Y hydroxide is between 10.5 and 11.5 [18]. This conclusion indicates that it is impossible to guarantee the complete precipitation of Y, Al and Nd at the same pH value during the preparation process of Nd:YAG precursors.…”
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