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“…Next, 1-(5-methyl-1-phenyl-1 H -1,2,3-triazol-4-yl)-3-phenylprop-2-en-1-one ( 15 ) [54] was reacted with 6-amino-2-thioxo-2,3-dihydropyrimidin-4(1 H )-one ( 16 ) in ethanol to afford 7-(5-methyl-1-phenyl-1 H -1,2,3-triazol-4-yl)-5-phenyl-2-thioxo-2,3-dihydropyrido[2,3- d ]pyrimidin-4(1 H )-one ( 17 ) in a good yield. Structure 17 was elucidated by elemental analysis, spectral data and chemical transformation.…”
Section: Resultsmentioning
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“…Next, 1-(5-methyl-1-phenyl-1 H -1,2,3-triazol-4-yl)-3-phenylprop-2-en-1-one ( 15 ) [54] was reacted with 6-amino-2-thioxo-2,3-dihydropyrimidin-4(1 H )-one ( 16 ) in ethanol to afford 7-(5-methyl-1-phenyl-1 H -1,2,3-triazol-4-yl)-5-phenyl-2-thioxo-2,3-dihydropyrido[2,3- d ]pyrimidin-4(1 H )-one ( 17 ) in a good yield. Structure 17 was elucidated by elemental analysis, spectral data and chemical transformation.…”
Section: Resultsmentioning
“…General Producer A mixture of 1 [27] (3.3 gm, 10 mmol) and the appropriate amount of malononitrile, acetylacetone and diethylmalonate (10 mmol) was heated under reflux in ethanol (20 mL) containing a catalytic amount of triethyamine (5-10 drops) for 3 h. The reaction mixture was cooled, and the solid formed was separated and recrystallized from the proper solvent to give the corresponding derivatives 2-4, respectively, in a good yield. and recrystallized from the proper solvent to give the corresponding compounds 13 and 14 respectively in a good yield.…”
Section: Synthesis Of Compounds 2-4mentioning
“…We are incorporated in a research group aimed to produce biologically active heterocyclic compounds using available chemicals [5,6,[23][24][25][26][27][28][29][30][31]. Our growing interest in this manuscript is incorporation between 1,2,3-triazole ring and pyrazoline ring in a new heterocyclic compound 1 [5].…”
Section: Introductionmentioning
“…Our results provide that the newly synthetic hybrid molecules could be targets for HCC treatment. Focusing on the aforementioned findings and in continuation of our aim to synthesize new pharmaceutically active compounds, 1,2,6,7,37−47 For the formation of products (3−9), it was suggested that the reaction proceeded via the condensation reaction between the acetyl group of compound (1) with the appropriate of the aldehydes (2a−g) to afford the corresponding chalcones, which then reacted with AcONH 4 to yield the corresponding imino derivatives, followed by tandem Michael addition of the active methylene group of (3−9) to give the nonisolable intermediates A. The latter underwent in situ auto-oxidation that was followed by tautomerization and formation of the final products (3−9) (Scheme 2).…”
Section: ■ Introductionmentioning