1996
DOI: 10.1002/(sici)1099-0739(199602)10:1<1::aid-aoc466>3.0.co;2-a
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Synthesis of 1-O-R-5-deoxy-?-D-ribofuranosides with (CH3)2As and (CH3)2As?O as substituents at the 5-position and a methyl or 2?,3?-dihydroxypropyl group as the aglycone in the 1-position

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Cited by 13 publications

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“…Consequently, appropriate analytical standards are available in only a few laboratories. Considering the lack of the arsenosugar standards, ES-MS-MS was applied to confirm the identity of the arsenosugars ( ).…”
Section: Resultsmentioning
confidence: 99%
“…The application of electrospray tandem mass spectrometry (ES-MS-MS) to the characterization of the arsenosugars in the HPLC fractions was to confirm its validity by HPLC-ICP-MS. For the MS-MS experiments, selected ion monitoring (SIM) was performed in the positive mode to determine the [M + H] + ion, and the fragmentary voltage was optimized for the maximum sensitivity. Each sample solution for analysis was prepared by the addition of an appropriate amount of methanol (50%) and formic acid (1%) ( ).…”
Section: Methodsmentioning
confidence: 99%
See 1 more Smart Citation
Exaggerated anticipatory anxiety is common in social anxiety disorder (SAD). Neuroimaging studies have revealed altered neural activity in response to social stimuli in SAD, but fewer studies have examined neural activity during anticipation of feared social stimuli in SAD. The current study examined the time course and magnitude of activity in threat processing brain regions during speech anticipation in socially anxious individuals and healthy controls (HC). Method Participants (SAD n = 58; HC n = 16) underwent functional magnetic resonance imaging (fMRI) during which they completed a 90s control anticipation task and 90s speech anticipation task.
“…Consequently, appropriate analytical standards are available in only a few laboratories. Considering the lack of the arsenosugar standards, ES-MS-MS was applied to confirm the identity of the arsenosugars ( ).…”
Section: Resultsmentioning
confidence: 99%
“…The application of electrospray tandem mass spectrometry (ES-MS-MS) to the characterization of the arsenosugars in the HPLC fractions was to confirm its validity by HPLC-ICP-MS. For the MS-MS experiments, selected ion monitoring (SIM) was performed in the positive mode to determine the [M + H] + ion, and the fragmentary voltage was optimized for the maximum sensitivity. Each sample solution for analysis was prepared by the addition of an appropriate amount of methanol (50%) and formic acid (1%) ( ).…”
Section: Methodsmentioning
confidence: 99%
Exaggerated anticipatory anxiety is common in social anxiety disorder (SAD). Neuroimaging studies have revealed altered neural activity in response to social stimuli in SAD, but fewer studies have examined neural activity during anticipation of feared social stimuli in SAD. The current study examined the time course and magnitude of activity in threat processing brain regions during speech anticipation in socially anxious individuals and healthy controls (HC). Method Participants (SAD n = 58; HC n = 16) underwent functional magnetic resonance imaging (fMRI) during which they completed a 90s control anticipation task and 90s speech anticipation task.
Exaggerated anticipatory anxiety is common in social anxiety disorder (SAD). Neuroimaging studies have revealed altered neural activity in response to social stimuli in SAD, but fewer studies have examined neural activity during anticipation of feared social stimuli in SAD. The current study examined the time course and magnitude of activity in threat processing brain regions during speech anticipation in socially anxious individuals and healthy controls (HC). Method Participants (SAD n = 58; HC n = 16) underwent functional magnetic resonance imaging (fMRI) during which they completed a 90s control anticipation task and 90s speech anticipation task.
Exaggerated anticipatory anxiety is common in social anxiety disorder (SAD). Neuroimaging studies have revealed altered neural activity in response to social stimuli in SAD, but fewer studies have examined neural activity during anticipation of feared social stimuli in SAD. The current study examined the time course and magnitude of activity in threat processing brain regions during speech anticipation in socially anxious individuals and healthy controls (HC). Method Participants (SAD n = 58; HC n = 16) underwent functional magnetic resonance imaging (fMRI) during which they completed a 90s control anticipation task and 90s speech anticipation task.