1996
DOI: 10.1002/(sici)1099-0739(199602)10:1<1::aid-aoc466>3.0.co;2-a
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Synthesis of 1-O-R-5-deoxy-?-D-ribofuranosides with (CH3)2As and (CH3)2As?O as substituents at the 5-position and a methyl or 2?,3?-dihydroxypropyl group as the aglycone in the 1-position
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Cited by 13 publications
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“…Consequently, appropriate analytical standards are available in only a few laboratories. Considering the lack of the arsenosugar standards, ES-MS-MS was applied to confirm the identity of the arsenosugars ( − ).…”
Section: Resultsmentioning
confidence: 99%
“…Consequently, appropriate analytical standards are available in only a few laboratories. Considering the lack of the arsenosugar standards, ES-MS-MS was applied to confirm the identity of the arsenosugars ( − ).…”
Section: Resultsmentioning
confidence: 99%
“…The application of electrospray tandem mass spectrometry (ES-MS-MS) to the characterization of the arsenosugars in the HPLC fractions was to confirm its validity by HPLC-ICP-MS. For the MS-MS experiments, selected ion monitoring (SIM) was performed in the positive mode to determine the [M + H] + ion, and the fragmentary voltage was optimized for the maximum sensitivity. Each sample solution for analysis was prepared by the addition of an appropriate amount of methanol (50%) and formic acid (1%) ( − ).…”
Section: Methodsmentioning
confidence: 99%
