Abstract:In this study, a new macrobicyclic ligand 3 with mixed donor atoms was synthesized starting from 27-membered macrocycle ligand 1 via the formation of novel N-pivot lariat ether 2. The characterization of the structures of new compounds 2 and 3 was realized by several spectroscopic techniques such as 1 H NMR, 13 C NMR, IR, UV-Vis, and MS. Besides, the extraction ability of ligands 2 and 3 was investigated using liquid-liquid extraction. On considering the extraction, the highest efficiency was observed for Ag(I… Show more
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