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“…Compounds 5 and 6 (n = 1-3) were synthesized according to the reported methods. 15 Finally, 1, 2, and 3 were prepared by the S N 2 reaction of 6 with dipicolylamine in the presence of Cs 2 CO 3 and KI in MeCN at 40°C. 16 First, the fluorescence emission changes (k ex = 335 nm, k em = 394 nm) of NIEDPA (1, 5 lM) according to the Zn 2+ (perchlorate salt) concentration were measured in 10 mM HEPES buffer (pH 7.4) at 25°C (Fig.…”
Section: Introductionmentioning
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“…Compounds 5 and 6 (n = 1-3) were synthesized according to the reported methods. 15 Finally, 1, 2, and 3 were prepared by the S N 2 reaction of 6 with dipicolylamine in the presence of Cs 2 CO 3 and KI in MeCN at 40°C. 16 First, the fluorescence emission changes (k ex = 335 nm, k em = 394 nm) of NIEDPA (1, 5 lM) according to the Zn 2+ (perchlorate salt) concentration were measured in 10 mM HEPES buffer (pH 7.4) at 25°C (Fig.…”
Section: Introductionmentioning
“…Recently, various methodologies for the generation of selenoaldehydes 3 have been reported in the light of their structural interests, their potentiality as new reactive intermediates for the organic reactions, and the increasing interests in the biological activities [1][2][3] for some selenoaldehydes. The synthetic methodologies for selenoaldehydes 3 are roughly classified to the five categories, i.e., (i) oxygen-selenium exchanging reactions of aldehydes [4][5][6][7][8][9][10][11][12][13], (ii) direct selenation of intermediary carbenes or carbenoids using elemental selenium [14][15][16], (iii) sigmatropic rearrangement of substituted alkenyl selenides [17], (iv) elimination of selenides bearing a suitable leaving group adjacent to the selenium atom [18][19][20][21], and (v) alkylation of stable selenoformate esters [22][23][24][25].…”
Section: Introductionmentioning
“…Temperature range for rt is 25 ± 2 °C. (1) [24]. A mixture of 1,8-naphthalic anhydride (4 g, 20.8 mmol) and 3-amino-1-propanol (1.86 mL, 24.6 mmol) in ethanol (40 mL) was heated under reflux for 5 h. The resulting mixture was concentrated by evaporating ethanol under reduced pressure to afford a solid residue, which was purified by column chromatography over silica gel (CH 2 Cl 2 /MeOH = 1:1) to afford compound 1 as an off-white solid (4.27 g, 83%).…”
Section: General Informationmentioning
“…To attach the N-mustard moiety to the naphathalimide core, we synthesized compound 2 from naphthalic anhydride [24,25]. Compound 2 was refluxed with an aminoalcohol in CH 3 CN to yield the key precursor compound 3, which was converted to compound 4 by refluxing in HCHO and HCOOH.…”
Section: Chemistrymentioning