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Cited by 32 publications
(16 citation statements)
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“…Materials and Equipment. The preparation of compounds 1 and 2 has been reported elsewhere . The compounds were stored in a refrigerated desiccator.…”
Section: Methodsmentioning
confidence: 99%
“…Materials and Equipment. The preparation of compounds 1 and 2 has been reported elsewhere . The compounds were stored in a refrigerated desiccator.…”
Section: Methodsmentioning
confidence: 99%
“…Finally, 7-dimethylamino benzo[f]isocoumarin 11c and 7-diethylamino benzo[f]isocoumarin 11d were obtained by catalytic reduction of nitro group of 11a to give the 7-amino benzo[f]isocoumarin 11b, followed by dialkylation of the amino group with alkyl iodide and potassium carbonate in DMSO at 65 °C 23 (Scheme 3). The reaction with ethyl iodide resulted slower and beside the desired product 11d, a small amount of the monoethylated derivative 11e was isolated.…”
Section: Scheme 2: Synthesis Of D--a Isocoumarins 1f-gmentioning
confidence: 99%
“…The exoisomer selectivity agrees with those reported previously for similar reactions. [34,36,37] The synthesis of the S-NB precursor was achieved by a similar procedure to the one used for L-NB. However, instead of treating 4 with cyclopentadiene to give the L-NB precursor, compound 4 was treated with quadricyclane to give the S-NB precursor.…”
Section: Introductionmentioning
confidence: 99%