volume 49, issue 1, P65-74 2007
DOI: 10.1002/jctb.280490107
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Abstract: The dimers and trimers of norbornadiene have a unique polycyclic strained structure and are of great practical value. A systematic study of the synthesis of norbornadiene j?om dicyclopentadiene and acetylene under pressure has been carried out. The efects of various operating parameters on product distribution have been determined. The optimum conditions for the synthesis are: (i) temperature, 290°C; (ii) residence period, 16 min; (iii) mole ratio of C2H2: N,: dicyclopentadiene, 1:1:0.4; and (iv) initial pres…

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