volume 44, issue 4, P644-646 1988
DOI: 10.1107/s0108270188000356
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Abstract: Abstract.[Ni(C,oH14N4S2)(H20)21 (NO3)2, Mr= 473.12, triclinic, Pi, a = 10.305 (2), b = 10.483 (2), c= 10.791 (2) A, a= 62.46 (1), fl= 64.66 (1), ~-65.22 (1) °, V= 897.9 (3) A 3, Z = 2, Dx= 1-750 g cm -a, 2(Mo Ka--) = 0.71073 ]k, p = 13.6 cm -1, F(000) = 448, T = 293 K, final R = 0.036 for 2666 observed reflections. The Ni n ion is octahedrally coordinated by two imidazole N atoms and two thioether S atoms of the ligand 1,6-bis(4-imidazolyl)-2,5-dithiahexane, and two O atoms of coordinating water molecules. Th…

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