Solid phase microextraction Arrow for the determination of synthetic musk fragrances in fish samples

Castro, Óscar; Trabalón, Laura; Schilling, Beat; Borrull, Francesc; Pocurull, Eva

doi:10.1016/j.chroma.2019.01.032

Cited by 22 publications

(4 citation statements)

References 24 publications

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“…To overcome these, many studies have focused in recent years on metals, such as gold, silver, platinum, titanium, copper, and stainless steel, as substrates for SPME fibers [11]. In addition, a growing trend in developing SPME coating deals with obtaining substrates with high corrosion resistance and high stability as well as high chemical activity and simple surface modification [12,13] (Table 1).…”

Section: Solid-phase Microextraction (Spme)mentioning

confidence: 99%

Comprehensive Strategy for Sample Preparation for the Analysis of Food Contaminants and Residues by GC–MS/MS: A Review of Recent Research Trends

Gao

Wang³

et al. 2021

Foods

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Food safety and quality have been gaining increasing attention in recent years. Gas chromatography coupled to tandem mass spectrometry (GC–MS/MS), a highly sensitive technique, is gradually being preferred to GC–MS in food safety laboratories since it provides a greater degree of separation on contaminants. In the analysis of food contaminants, sample preparation steps are crucial. The extraction of multiple target analytes simultaneously has become a new trend. Thus, multi-residue analytical methods, such as QuEChERs and adsorption extraction, are fast, simple, cheap, effective, robust, and safe. The number of microorganic contaminants has been increasing worldwide in recent years and are considered contaminants of emerging concern. High separation in MS/MS might be, in certain cases, favored to sample preparation selectivity. The ideal sample extraction procedure and purification method should take into account the contaminants of interest. Moreover, these methods should cooperate with high-resolution MS, and other sensitive full scan MSs that can produce a more comprehensive detection of contaminants in foods. In this review, we discuss the most recent trends in preparation methods for highly effective detection and analysis of food contaminants, which can be considered tools in the control of food quality and safety.

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Section: Solid-phase Microextraction (Spme)mentioning

confidence: 99%

Comprehensive Strategy for Sample Preparation for the Analysis of Food Contaminants and Residues by GC–MS/MS: A Review of Recent Research Trends

Gao

Wang³

et al. 2021

Foods

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show abstract

“…In addition, similar to SPME, SPME Arrow can be fully automated. Therefore, SPME Arrow is more advantageous for analyzing volatile substances in various types of foods [ 32 , 33 ].…”

Section: Introductionmentioning

confidence: 99%

Analysis of Volatile Compounds in Soju, a Korean Distilled Spirit, by SPME-Arrow-GC/MS

Cha

Chin

Lee

et al. 2020

Foods

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The SPME Arrow technology—a novel solid phase micro-extraction technique—was used to analyze Soju, a traditional Korean distilled liquor, in barrels made of Quercus spp. The volatile compounds detected when the barrels were toasted were analyzed. Five types of sorbents—carbon wide range/polydimethylsiloxane, divinylbenzene/carbon wide range/polydimethylsiloxane, divinylbenzene/polydimethylsiloxane, polydimethylsiloxane, and polyacrylate—were used for this investigation. Fifty-four volatile compounds were detected in Soju using gas chromatography/mass spectrometry. A high extraction efficiency was obtained using carbon wide range/polydimethylsiloxane. Nineteen samples were analyzed using barrels made of six species of carbonated oak (Q. aliena, Q. variabilis, Q. dentate, Q. acutissima, Q. mongolica, and Q. serrata) and control groups in three ways: noncharring, medium charring, and heavy charring. Ethanol, 1-propanol, isoamyl acetate, and isoamyl alcohol can be used as indicator volatile components for Soju and other such traditional Korean distilled liquors. We believe our study results can be used to design better analysis methods for Soju and other distilled liquors.

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“…Novel geometry of SPME, like the thin-film microextraction blades (TF-SPME) [18] or biocompatible surface coated probes (BSCP) [21,22] have been also developed to provide higher sensitivity and reduced analysis time due both to the high surface area-to-volume ratio and to the possibility of a direct mass spectrometry (MS) coupling. In this context, many ex vivo SPME studies could be implemented for in vivo applications, in order to capture short-living and labile compounds, avoiding sample degradation [10,[23][24][25][26][27].…”

Section: Introductionmentioning

confidence: 99%

Recent Advances in In Vivo SPME Sampling

et al. 2020

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In vivo solid-phase microextraction (SPME) has been recently proposed for the extraction, clean-up and preconcentration of analytes of biological and clinical concern. Bioanalysis can be performed by sampling exo- or endogenous compounds directly in living organisms with minimum invasiveness. In this context, innovative and miniaturized devices characterized by both commercial and lab-made coatings for in vivo SPME tissue sampling have been proposed, thus assessing the feasibility of this technique for biomarker discovery, metabolomics studies or for evaluating the environmental conditions to which organisms can be exposed. Finally, the possibility of directly interfacing SPME to mass spectrometers represents a valuable tool for the rapid quali- and quantitative analysis of complex matrices. This review article provides a survey of in vivo SPME applications focusing on the extraction of tissues, cells and simple organisms. This survey will attempt to cover the state-of- the-art from 2014 up to 2019.

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Solid phase microextraction Arrow for the determination of synthetic musk fragrances in fish samples

Cited by 22 publications

References 24 publications

Comprehensive Strategy for Sample Preparation for the Analysis of Food Contaminants and Residues by GC–MS/MS: A Review of Recent Research Trends

Comprehensive Strategy for Sample Preparation for the Analysis of Food Contaminants and Residues by GC–MS/MS: A Review of Recent Research Trends

Analysis of Volatile Compounds in Soju, a Korean Distilled Spirit, by SPME-Arrow-GC/MS

Recent Advances in In Vivo SPME Sampling

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