2021
DOI: 10.1039/d0dt04200e
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Abstract: The crucial role of solubilization and crystallization steps in the vibrational and optical properties of {Ta6Bri12} cluster core containing systems.

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Cited by 11 publications
(45 citation statements)
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“…The K4[{Nb6−xTaxX i 12}X a 6] (X = Cl, Br; 0 ≤ x ≤ 6) cluster compounds were prepared by solid-state chemistry using an optimized method derived from that of F. W. Koknat et al, and Wilmet et al [5][6][7]. Potassium chloride (KCl; Alfa Aesar-99%, Haverhill, MA, USA), ] n−/+ cluster unit (Blue = M; red = X i ; green = X a ).…”
Section: Methodsmentioning
confidence: 99%
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“…The K4[{Nb6−xTaxX i 12}X a 6] (X = Cl, Br; 0 ≤ x ≤ 6) cluster compounds were prepared by solid-state chemistry using an optimized method derived from that of F. W. Koknat et al, and Wilmet et al [5][6][7]. Potassium chloride (KCl; Alfa Aesar-99%, Haverhill, MA, USA), ] n−/+ cluster unit (Blue = M; red = X i ; green = X a ).…”
Section: Methodsmentioning
confidence: 99%
“…The K 4 [{Nb 6−x Ta x X i 12 }X a 6 ] (X = Cl, Br; 0 ≤ x ≤ 6) cluster compounds were prepared by solid-state chemistry using an optimized method derived from that of F. W. Koknat et al, and Wilmet et al [5][6][7]. Potassium chloride (KCl; Alfa Aesar-99%, Haverhill, MA, USA), potassium bromide (KBr; Acros-99%, Waltham, MA, USA), niobium pentachloride (NbCl 5 ; Strem-99.99%, Newburyport, MA, USA), niobium pentabromide (NbBr 5 ; Strem-99.9%), tantalum pentachloride (TaCl 5 ; Alfa Aesar-99.8%), tantalum pentabromide (TaBr 5 ; Alfa-99.9%), niobium powder (Alfa Aesar-99.8%) and tantalum powder (Alfa Aesar-99.97%) were used as starting precursors.…”
Section: Methodsmentioning
confidence: 99%
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