Soil and water samples collected biweekly over 2 month period, starting from 15 May to 30 June 2005 from Syrian costal area were analyzed to determine the occurrence of Pesticides residues and mainly the organochlorine pesticides. None of the conventional pesticides were detected neither in soil nor in water samples, the only insecticides were detected in the samples were the organoclorine insecticides. In water samples, the DDT and it is breakdown products of DDE was detected only in some sampling interval in both coastal governorates Tartous, and Latakia, and concentration typically ranged from 0.0018 to 0.0085 mg/L whereas, the 4,4 DDD were almost found in all water samples and ranged from 0.0076 to 0.0705 mg/L. Lindane, and δ BHC were detected in all samples of both governorates at concentration ranged from 0.0202 to 0.0537 and from 0.0106 to 0.136 mg/L respectively. In soil the results showed that, the high level of Lindan residues in all analyzed samples in both governorates. Concentration typically ranged from 8.54 to 22.50 mg/kg, and that was due to the more recent banning of Lindan (in 2000). The residue levels of DDE were the highest among the rest of the detected OC residues and it ranged from 8.54 to 22.50. However the range of residues concentration of the other detected OC. Pesticides were as follow; 4,4 DDD from 3.81 to 14.37, 4,4 DDT from 2,22 to 12.38, 2,4 DDT from 2.94 to 5.28, HCH from 3.18 to 571, 2,4 DDD from 0.87 to 4.28 and the combination of Endosulfan and Endosulfan sulfate ranged from 0.05 to 9.18 mg/kg.