Pd‐Catalyzed Threefold Arylation of Baylis–Hillman Bromides and Acetates with Triarylbismuth Reagents

Rao, Maddali L. N.; Giri, Somnath

doi:10.1002/ejoc.201200543

Cited by 19 publications

(3 citation statements)

References 76 publications

(25 reference statements)

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“…Purification by column chromatography (eluant: pentane/diethyl ether 9:1) afforded 20 mg of 7m (colorless oil, 39% yield). The spectroscopic data of 7m were in accordance with the literature …”

Section: Methodssupporting

confidence: 78%

“…IR (NaCl, ν cm −1 ): 2963, 2866, 1515, 898. GC-MS (m/z): 250 (M + , 5), 236 (9), 235 (48), 194 (28), 193 (100), 192 (52), 117 (38), 115 (47). Anal.…”

Section: ■ Experimental Sectionmentioning

confidence: 99%

“…The spectroscopic data of 7m were in accordance with the literature. 47 The Journal of Organic Chemistry ■ ASSOCIATED CONTENT…”

Section: The Journal Of Organic Chemistrymentioning

confidence: 99%

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Visible Light Promoted Metal- and Photocatalyst-Free Synthesis of Allylarenes

et al. 2017

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The metal- and photocatalyst-free synthesis of substituted allylarenes has been carried out under visible light driven conditions. The process was based on the photogeneration of aryl radicals from arylazo sulfones and their ensuing reaction with allyl sulfones. The developed procedure was very efficient when using substrates bearing electron-withdrawing groups, and allowed for the preparation of α-benzyl styrenes and 2-benzyl acrylates in good yields.

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Section: Methodssupporting

confidence: 78%

“…IR (NaCl, ν cm −1 ): 2963, 2866, 1515, 898. GC-MS (m/z): 250 (M + , 5), 236 (9), 235 (48), 194 (28), 193 (100), 192 (52), 117 (38), 115 (47). Anal.…”

Section: ■ Experimental Sectionmentioning

confidence: 99%