2007
DOI: 10.1002/chin.200740167
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Armando Carlone,
Giuseppe Bartoli,
Marcella Bosco
et al.

Abstract: Organo-phosphorus compounds S 0080Organocatalytic Asymmetric Hydrophosphination of α,β-Unsaturated Aldehydes. -Highly enantioenriched air-stable (hydroxypropyl)diphenylphosphine-borane adducts (III), (V) and (VII) are formed by a sequential one-pot reaction involving the addition of diphenylphosphine to α,β-unsaturated aldehydes under catalysis of optically active proline derivative PYR and a benzoic acid, followed by reduction of the aldehyde group in the presence of excess NaBH4. Amino-phosphine-borane comp…

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