Vibroacoustic metamaterials offer an approach for the targeted damping of unwanted structural vibrations and noise by integrating periodically arranged resonators into a matrix of bulk material. Fabrication using the Laser Bed Powder Fusion (L‐PBF) process allows the targeted integration of bulk resonators and powder depots, leading to an extension of the designable damping properties. In this work, we focus on the adaptation of acoustic methods to characterize the properties of metamaterial plates. The investigated vibroacoustic metamaterial plates are made of nylon PA 1.2, combining material and structural damping. We investigated the vibration behavior of the plates over a range of frequencies using acoustic impedance measurements in a custom‐built measurement tube and compared it with structural dynamics experiments using an electrodynamic shaker. The measurements allow for the identification of stop bands (frequency range with high damping) and influencing factors such as metamaterial design, mass, powder amount and surface on the frequency dependent damping properties. The adapted technique investigated in this work provides an experimental platform to characterize the complex interplay of acoustic metamaterial design and holds promise for scaling up metamaterial technology for industrial applications due to its simplicity, small space requirement, and low cost.This article is protected by copyright. All rights reserved.