2004
DOI: 10.1016/j.mseb.2004.03.024
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Nickel and nickel oxide nanoparticles prepared from nickel nitrate hexahydrate by a low pressure spray pyrolysis

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Cited by 128 publications
(45 citation statements)
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“…Figure 4(a) reveals XRD peak values at 42 ∘ and 49 ∘ , which are associated with the (111) and (200) planes of orientation, respectively. These values correspond well to the typical diffraction patterns observed for face-centered cubic (fcc) Ni nanoparticles [27,28]. Similar results have been reported by Harish and coworker during the formation of nickel hydroxide nanoparticles [29].…”
Section: Xrd and Tem Analysis Of Intradendrimer Ni(0) Particlessupporting
confidence: 89%
“…Figure 4(a) reveals XRD peak values at 42 ∘ and 49 ∘ , which are associated with the (111) and (200) planes of orientation, respectively. These values correspond well to the typical diffraction patterns observed for face-centered cubic (fcc) Ni nanoparticles [27,28]. Similar results have been reported by Harish and coworker during the formation of nickel hydroxide nanoparticles [29].…”
Section: Xrd and Tem Analysis Of Intradendrimer Ni(0) Particlessupporting
confidence: 89%
“…On the other hand, reduced droplet size can be achieved either by using an electrospray which is capable of producing directly nanoscale monodispersed particles or by the modification of atomizing techniques, like filter expansion aerosol generator (FEAG) assisted spray pyrolysis (FEAG-SP) [35]. The low-pressure condition was applied in spray pyrolysis as an attempt to control the environment of the surrounding processes as reported by Wang et al [36], in the investigation of low pressure-SP (LPSP). Furthermore, the development of SP method was based on the diversity of thermal energy behavior as a heat source such as flame-SP (FSP) [37] and pulse combustion SP [38].…”
Section: Spray Pyrolysismentioning
confidence: 99%
“…Generally, a onedroplet-to-one-product particle (ODOP) conversion is considered the typical particle formation mechanism in conventional spray pyrolysis (CSP). In this project, various modified spray pyrolysis methods were developed and introduced for nanoparticle synthesis, including salt-assisted spray pyrolysis (SASP) [9][10][11][12] and low pressure spray pyrolysis (LPSP) [13][14][15][16][17][18] as well as flame-assisted spray pyrolysis (FASP). [19][20] Salt-assisted spray pyrolysis (SASP) is a modified spray pyrolysis method that introduces salts into the precursor solution.…”
Section: Nanoparticle Synthesis Technologiesmentioning
confidence: 99%
“…Low-pressure spray pyrolysis (LPSP) was applied to the proper nanoparticle synthesis as well. [13][14][15][16] The distinguishing feature of this process is a dramatically different particle formation mechanism. It is expected that a micron-sized droplet will first undergo rapid solvent evaporation upon entering the low-pressure environment.…”
Section: Nanoparticle Synthesis Technologiesmentioning
confidence: 99%
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