The levels of selected metals (Ca, Na, Mg, Fe, Cu, Pb, Ni, Co, Cr and Cd) were determined in effluent, groundwater and soil samples obtained from surgical instrument industries in Sialkot Pakistan by AAS. The metal distribution in the three media was quite divergent with high skewness and standard deviation parameters. These industries indiscriminately discharge the metal laden effluents to nearby lands and freshwater resources. Thus, soil adjacent to these industries exhibited Fe as the major contributor. The multiple correlations in terms of effluent versus soil correlation coefficient matrix evidenced that Ni, Mg, Cr and Cd in the soil originated from the effluents. Multivariate analysis (Principal component analysis and cluster analysis) also confirmed the contamination of soil and groundwater to be rising from surgical industry effluents.