1997
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Abstract: The binding of the host H1 (N,N′-bis(6-pivalamidopyrid-2-yl)-3,5-pyridinedicarboxamide) to three different ruthenium polypyridine complexes with an attached barbituric acid and barbital moieties (RuG1, RuG2, RuG3) (where G1 ) 5-[4-(4′-methyl)-2,2′-bipyridylidene]-2,4,6-(1H,3H,5H)-pyrimidinetrione, G2 ) 5-[4-(4′-methyl)-2,2′bipyridyl]methyl-2,4,6-(1H,3H,5H)-pyrimidinetrione, and G3 ) 5-ethyl, 5-[4-(4′-methyl)-2,2′-bipyridyl]methyl-2,4,6-(1H,3H,5H)-pyrimidinetrione) and Ru ) (4,4′-di-tert-butyl-bpy) 2 Ru (bpy ) … Show more

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“…1(b)] as it binds to the hosts in solvents such as CH 2 Cl 2 , d-CHCl 3 , d 3 -CH 3 CN and d 6 -DMSO. 12 The host molecules are derivatives of 2,6-diaminopyridine amides which are assembled from the reaction of the appropriate 2,6-diaminopyridine derivative with 3,5-pyridinedicarboxylic acid chloride. Two different amino hosts, 3,5-bis[(6-aminopyrid-2-yl)amino]carbonylpyridine and 3,5-bis[(6-amino-4-isopropoxypyrid-2-yl)-amino]carbonylpyridine, were used.…”
Section: Synthesis and Characterization Of Guest And Host Moleculesmentioning
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“…1(b)] as it binds to the hosts in solvents such as CH 2 Cl 2 , d-CHCl 3 , d 3 -CH 3 CN and d 6 -DMSO. 12 The host molecules are derivatives of 2,6-diaminopyridine amides which are assembled from the reaction of the appropriate 2,6-diaminopyridine derivative with 3,5-pyridinedicarboxylic acid chloride. Two different amino hosts, 3,5-bis[(6-aminopyrid-2-yl)amino]carbonylpyridine and 3,5-bis[(6-amino-4-isopropoxypyrid-2-yl)-amino]carbonylpyridine, were used.…”
Section: Synthesis and Characterization Of Guest And Host Moleculesmentioning
“…12 An increase in the fluorescence intensity of the RuG2 upon binding of the different hosts was used to calculate the 1:1 binding constants. Fluorescence methods were used mainly in CH 2 Cl 2 , where the large binding constants observed required the use of low concentrations of RuG2 and host molecules.…”
Section: Binding Studies Of Rug2 To Different Hostsmentioning
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“…1 Substitutions at the 4-, 5-and 6-positions of the bipyridine framework have been actively investigated over the last three decades, resulting in a wide range of new derivatives that find applications in macromolecular chemistry, 2 catalysis, 3 molecular recognition, 4 and optoelectronics. 5 In addition, this family of ligands has been incorporated into the structures of molecular sensors, 6 metal organic frameworks 7 and luminescent devices.…”
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