Microwave-assisted synthesis and characterization of 3D flower-like Bi2S3 superstructures

Low‐temperature urea‐assisted hydrothermal synthesis of Bi2S3 nanostructures with different morphologies

“…No tubular morphology could be found. Using (NH 2 ) 2 CS as the sulfur source to control the morphological evolution of metal sulfides in the solution phase has been intensively studied [20][21][22][23][24]. It is well known that thiourea (Tu) coordinates to bismuth ions to form Bi 3+ -(Tu) n complexes, prevents the explosive production of bismuth sulfide and benefits the oriented growth of final nanorods.…”

Synthesis and Characterization PbS and Bi2S3 Nanostructures via Microwave Approach and Investigation of Their Behaviors in Solar Cell

“…Bi 2 S 3 has potential applications including photovoltaics [5], IR spectroscopy [6] and thermoelectrics [7,8]. Many techniques including hydrothermal [9,10] solvothermal [11][12][13] biomolecule assisted method [14] thermal decomposition, ionic liquid-assisted templating route [15], photochemical synthesis method [16], sonochemical [17], template-synthesis methods [18] and microwave [19] have been applied to prepare Bi 2 S 3 nanoparticles or superstructures. Bi 2 S 3 nanostructures with different morphologies, such as nanorods [20] nanotubes [21], flower-like structures [22], nanoribbions [23] and nanowire [24], have been synthesized.…”

Synthesis of different morphologies of bismuth sulfide nanostructures via hydrothermal process in the presence of thioglycolic acid

“…In the recent several years, many methods have been exploited to prepare nanostructured Bi 2 S 3 with different morphologies, such as ultrasonic chemistry method [10], microwave-assisted route [11,12], photochemical synthesis method [13,14], high temperature thermal decomposition of single-source precursors [15,16], ionic liquid-assisted templating route [17], hydrothermal [18,19] and solvothermal methods [20][21][22]. However, most of the techniques mentioned above need relatively higher temperature and pressure, or the preparation procedures are complex.…”