Micro-solid-phase extraction

Naing, Nyi Nyi; Tan, Sze Chieh; Lee, Hian Kee

doi:10.1016/b978-0-12-816906-3.00016-9

Cited by 14 publications

(11 citation statements)

References 94 publications

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“…3 This result renders mTpBD-Me 2 -1 : 1.25 appropriate for the proposed application, since efficiency values over 65% are set as satisfactory for micro-solid phase extraction procedures in static mode. 53 An increase in the initial concentration of OA to 15, 50, and 100 μM led to an increase in the amount adsorbed by mTpBD-Me 2 -1 : 1.25 from q t = 9 mg g −1 to q t = 61 mg g −1 (Fig. S10 †), showing the excellent adsorption capacity of the sorbent for OA, and indicating that at these concentrations saturation of the adsorbent was not yet reached.…”

Section: †)mentioning

confidence: 97%

One-step synthesis of magnetic covalent organic framework composite for the adsorption of marine toxin okadaic acid

et al. 2023

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Section: †)mentioning

confidence: 97%

One-step synthesis of magnetic covalent organic framework composite for the adsorption of marine toxin okadaic acid

et al. 2023

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“…Micro-SPE (µ-SPE) has been used in many studies in reference to the trend towards miniaturization, with the "µ" designation intended to imply a reduction in device dimensions, amount of sorbents, and/or use of microsized or nanosized materials (particularly the latter with their advantageously large surface area and exceptional physicochemical properties) [96]. In comparison to standard SPE, µ-SPE provided substantial insight into sample preparation that reduces the solvents' operating time and chemical consumption.…”

Section: Micro-solid Phase Extractionmentioning

confidence: 99%

“…Therefore, µ-SPE has several benefits, including low solvent consumption, a higher enrichment factor than SPME, extremely high selectivity and sensitivity, simplicity of application, being less time consuming, a relatively low cost, compatibility with various systems of analyte separation and detection, and also enabling headspace and immersion modes. Despite all of this, there are drawbacks to the implementation of µ-SPE, including analyte carry-over, fragile fibres, and a stationary phase with a restricted range [60,95,96].…”

Section: Micro-solid Phase Extractionmentioning

confidence: 99%

Miniaturized Solid Phase Extraction Techniques Applied to Natural Products

et al. 2023

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Natural products are increasingly becoming part of our daily lives through their use in industry, food, as therapeutic agents, etc. To evaluate their possible applications, it is essential to characterize them chemically to explore their potential. Different techniques may be used to characterize natural products, including microextraction techniques. These techniques have been gaining popularity due to the advantages associated with their low use of organic solvents and the small amount of sample used relative to more classical sample preparation techniques. Their application in the extraction of compounds from natural products is still scarce. This manuscript intends to review the most used solid-based miniaturized sample preparation techniques applied to determining compounds in natural products. The main applications of these methodologies will be discussed, with a particular focus on natural product analysis, as well as their advantages and disadvantages over traditionally used sample preparation techniques.

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“…In a generic term, Micro Solid Phase Extraction (μ-SPE) has been used when a reduced amount of sorbents, and/or microsized or nanosized materials were applied for the extraction [54]. There are several μ-SPE techniques reported in the literature, including Dispersive Micro Solid Phase Extraction (D-μ-SPE), membrane protected micro solid phase extraction (MP-μ-SPE), pipette tip micro solid phase extraction (PT-μ-SPE) and spin column micro solid phase extraction (SC-μ-SPE).…”

Section: Microextraction Techniques Based On Solid Sorbentsmentioning

confidence: 99%

Critical review on microextraction techniques used in determination of histamine in food samples

et al. 2022

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Biogenic amines are basic nitrogen compounds, which are formed due to the decarboxylation of amino acids or/and the amination and the transformation of aldehydes and ketones. Histamine is a heterocyclic biogenic amine present in a wide range of food products, including fish and fishery products, meat and their products, and other dairy products and beverages. The present review summarizes the innovative sample preparation methods for the extraction of histamine from various sample matrices. Both solid phase and liquid phase based microextraction techniques are used for extracting histamine, but the latter ones are the most popular. Currently, all the sample preparation techniques for the histamine extraction fulfil the demand of green chemistry standards. These sample preparation procedures are presented in the present review along with their special features, advantages and disadvantages. Graphical Abstract

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Micro-solid-phase extraction

Cited by 14 publications

References 94 publications

One-step synthesis of magnetic covalent organic framework composite for the adsorption of marine toxin okadaic acid

One-step synthesis of magnetic covalent organic framework composite for the adsorption of marine toxin okadaic acid

Miniaturized Solid Phase Extraction Techniques Applied to Natural Products

Critical review on microextraction techniques used in determination of histamine in food samples

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