N-Benzyl-2-hydroxyethanaminium cyanurate

Abstract

In the cation of the title compound C9H14ON+·C3H2O3N3 −, the benzyl­amine C—N bond subtends a dihedral angle of 78.3 (2)° with the phenyl ring. The cyanurate anion is in the usual keto-form and shows an r.m.s. deviation from planarity of 0.010 Å. In the crystal, the cyanurate anions form N—H⋯O hydrogen-bonded zigzag ribbons along [001]. These ribbons are crosslinked by the organocations via O—H⋯N and N—H⋯O hydrogen bonds, forming bilayers parallel to (010) which are held together along [010] by slipped π–π inter­actions between pairs of cyanurate anions [shortest contact distances C⋯C = 3.479 (2), O⋯N = 3.400 (2); centroid–centroid distance= 4.5946 (9) Å] and between cyanurate and phenyl rings [centroid–centroid distance = 3.7924 (12) Å, ring–ring angle = 11.99 (10)°].

Hydrogen-Bonded Anionic Host Lattices Constructed with Isocyanurate and Thiourea/Urea

“…Interestingly, the thiourea sulfur atom does not participate in the construction of the host lattice, which is not usually observed among the known inclusion compounds of thiourea. A similar example can be found in the inclusion compound of 5-nitrobarbiturate, 2 15 Crystal Structure of (…”

“…Generation of the mono-, di-, and trianionic forms at p K a values of 6.85, 10.91, and >12, respectively, was reported by Aoki et al in 2000 . Surprisingly, to date only 12 single-crystal X-ray structures of hydrogen-bonded complexes of the ordered isocyanurate ion are documented in the Cambridge Structural Database, CSD V5.36 (November, 2014) with May 2015 update. − …”

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