“…A report of the synthesis of S-chloro-N,N-diethylthiohydroxylamine by chlorination of N,N-diethylthiohydroxylamine [7] is in error. The authors refer to a procedure described in Houben-Weyl [8], but the chloro compound in fact emerges as the product of the reaction between chlorine and N,N'-bis-(diethylamino)-disulfide.…”