ESI-MS reveals preferential complex formation of carbohydrates with <i>Z</i>-sinapinic acid compared with the <i>E</i>-isomer

León, Tobías Schmidt De; Salum, María Laura; Matsushita, Yasuyuki; Fukushima, Kazuhiko; Monge, Marı́a Eugenia; Erra‐Balsells, Rosa

doi:10.1039/d2nj02789e

New J. Chem.

2022

DOI: 10.1039/d2nj02789e

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ESI-MS reveals preferential complex formation of carbohydrates with Z-sinapinic acid compared with the E-isomer

Tobías Schmidt De León

María Laura Salum

Yasuyuki Matsushita

et al.

Abstract: Cinnamic acid derivatives including 3,5-dimethoxy-4-hydroxycinnamic acid, also referred to as sinapinic acid (SA), are efficient matrices used in matrix assisted laser desorption/ionization mass spectrometry (MALDI-MS). Previous findings have shown that...

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Analysis of carbohydrates and glycoconjugates by matrix‐assisted laser desorption/ionization mass spectrometry: An update for 2021–2022

Harvey

2024

Mass Spectrometry Reviews

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The use of matrix‐assisted laser desorption/ionization (MALDI) mass spectrometry for the analysis of carbohydrates and glycoconjugates is a well‐established technique and this review is the 12th update of the original article published in 1999 and brings coverage of the literature to the end of 2022. As with previous review, this review also includes a few papers that describe methods appropriate to analysis by MALDI, such as sample preparation, even though the ionization method is not MALDI. The review follows the same format as previous reviews. It is divided into three sections: (1) general aspects such as theory of the MALDI process, matrices, derivatization, MALDI imaging, fragmentation, quantification and the use of computer software for structural identification. (2) Applications to various structural types such as oligo‐ and polysaccharides, glycoproteins, glycolipids, glycosides and biopharmaceuticals, and (3) other general areas such as medicine, industrial processes, natural products and glycan synthesis where MALDI is extensively used. Much of the material relating to applications is presented in tabular form. MALDI is still an ideal technique for carbohydrate analysis, particularly in its ability to produce single ions from each analyte and advancements in the technique and range of applications show little sign of diminishing.

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Analysis of carbohydrates and glycoconjugates by matrix‐assisted laser desorption/ionization mass spectrometry: An update for 2021–2022

Harvey

2024

Mass Spectrometry Reviews

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show abstract

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ESI-MS reveals preferential complex formation of carbohydrates with Z-sinapinic acid compared with the E-isomer

Abstract: Cinnamic acid derivatives including 3,5-dimethoxy-4-hydroxycinnamic acid, also referred to as sinapinic acid (SA), are efficient matrices used in matrix assisted laser desorption/ionization mass spectrometry (MALDI-MS). Previous findings have shown that...

Cited by 1 publication

References 42 publications

Analysis of carbohydrates and glycoconjugates by matrix‐assisted laser desorption/ionization mass spectrometry: An update for 2021–2022

Analysis of carbohydrates and glycoconjugates by matrix‐assisted laser desorption/ionization mass spectrometry: An update for 2021–2022

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