Direct observations of multi-cyclic nanoindentation-induced phase transformations in single-crystal Ge

Kosai, Koji; Yan, Jiwang

doi:10.1088/2053-1591/ab1986

Cited by 2 publications

(1 citation statement)

References 35 publications

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“…However, most previous indentation studies focused on individual indentations, thus the effects of incremental-load cyclic loading/unloading still remains unknown. In recent years, cyclic indentation has been attempted on brittle singlecrystalline materials such as silicon [16,17] and germanium [18,19], and it was demonstrated that multi-cyclic indentation induced completely different mechanical responses from that of individual indentations. For optical glasses, multi-cyclic indentation tests were performed by using Vickers indenters [20] and spherical indenters [21] to investigate fatigue properties, and the evolution of indentation-induced cracks during cyclic bending tests was also investigated [22].…”

Section: Introductionmentioning

confidence: 99%

Crack Propagation Behavior of Fused Silica during Cyclic Indentation under Incremental Loads

2022

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Fused silica is an important optical material with important applications, where the surface must be precisely machined without subsurface damage. In this study, multi-cyclic indentations under incremental loads were performed on fused silica using two kinds of indenters to clarify the mechanisms of crack generation and propagation induced by precision grinding. It was found that incremental loading cyclic nanoindentation induced various patterns of subsurface cracking and surface spalling. Four kinds of surface spalling were identified at different locations around an indent, the temporal formation mechanisms of which were clarified by microscopic observation and topographical measurement. Load–displacement curve analysis demonstrated that incremental propagation of lateral cracks during early indentation cycles caused large-scale brittle fractures during later cycles. Compared with a Berkovich indenter, a cube-corner indenter caused more significant brittle fractures and surface spalling. The findings in this study will deepen the understanding of subsurface damaging mechanism of fused silica and other brittle solids caused by cyclic tool-workpiece interactions in grinding and other mechanical machining processes.

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