2020
DOI: 10.1515/ncrs-2020-0371
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Abstract: C12H17N3S, monoclinic, P21/c (no. 14), a = 9.3084(19) Å, b = 7.9523(16) Å, c = 16.905(3) Å, β = 92.26(3)°, V = 1250.4(4) Å3, Z = 4, Rgt(F) = 0.0330, wRref(F2) = 0.0914, T = 100(2) K.

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Cited by 3 publications
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“…Each of these is a Nmethyl species, i.e. MeN(H)C( S)N(H)N C(Me)CH 2 -CH 2 Ar, one with Ar = phenyl (Tan, Kwong et al, 2020a) and the other with Ar = 4-methoxybenzene (Tan et al, 2012). In the former, the molecule has a distinctive U-shaped conformation with a twist about the CH 2 -CH 2 bond [the C i -C m -C m -C p (i = imine, m = methylene, p = phenyl) torsion angle = À62.76 (16) ], a conformation stabilized, at least in part, by an intramolecular amine-N-HÁ Á Á(phenyl) interaction.…”
Section: Database Surveymentioning
confidence: 99%
“…Each of these is a Nmethyl species, i.e. MeN(H)C( S)N(H)N C(Me)CH 2 -CH 2 Ar, one with Ar = phenyl (Tan, Kwong et al, 2020a) and the other with Ar = 4-methoxybenzene (Tan et al, 2012). In the former, the molecule has a distinctive U-shaped conformation with a twist about the CH 2 -CH 2 bond [the C i -C m -C m -C p (i = imine, m = methylene, p = phenyl) torsion angle = À62.76 (16) ], a conformation stabilized, at least in part, by an intramolecular amine-N-HÁ Á Á(phenyl) interaction.…”
Section: Database Surveymentioning
confidence: 99%