Crystal structure and Hirshfeld surface analysis of 2,4,6,11-tetrakis(4-fluorophenyl)-9-oxa-1,5-diazatricyclo[5.3.1.0^3.8]undecane

Abstract

The compound, prepared by the NaBH4 reduction of 4,8,9,10-tetra­kis­(4-fluoro­phen­yl)-1,3-di­aza­adamantan-6-one in chloro­form and ethanol as solvent, crystallizes in the monoclinic space group P21/n with four mol­ecules in the unit cell.

Unprecedented synthesis, 1D, and 2D NMR spectral studies of 2,4,6,11‐tetraaryl‐9‐oxa‐1,5‐diazatricyclo[5.3.1.03.8] undecane via a novel rearrangement

“…Finally, the structure of 3e is unambiguously confirmed by single crystal X‐ray analysis (Figure ). Recently, we have published the crystal structure and Hirshfeld surface analysis of compound 3e in Acta Cryst E …”