volume 30, issue 43, Pno-no 2010
DOI: 10.1002/chin.199943007
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Ulrich Kortz,
Yves P. Jeannin,
Andre Teze
et al.

Abstract: A Novel Dimeric Ni-Substituted β-Keggin Silicotungstate: Structure and Magnetic Properties of-The title compound crystallizes in the monoclinic space group P2 1 /n with Z = 4 (single crystal XRD). The novel polyoxoanion of (III) consists of two [β-SiNi 2 W 10 O 36 (OH) 2 (H 2 O)] Keggin moieties linked via two bridging OH groups, leading to a planar Ni 2 (OH) 2 unit. The two half-units are related by an inversion center and each contains one Ni atom in the rotated triad. The central Ni 4 unit exhibits ferroma…

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