A study of the morphology of nickel electrodeposits and the influence of substrate and electrolyte, using high resolution replication

Application of a GaPO4 Crystal Microbalance for the Detection of Coke Formation in High-Temperature Reactors and Solid Oxide Fuel Cells

“…For the carbon deposition study, Ni was electrodeposited onto the Pt electrodes using a Watts bath consisting of a solution of 0.647 M H 3 BO 3 , 0.285 M NiSO 4 ·6H 2 O, and 0.047 M NiCl 2 ·6H 2 O. , Nitrogen was bubbled through the solution to rid the chamber of oxygen as well as being used during the plating experiments to rid the sample surface of H 2 bubbles formed. Nickel was used as the counter electrode together with a Hg/Hg 2 Cl 2 (SCE) reference electrode.…”

Application of a GaPO4 Crystal Microbalance for the Detection of Coke Formation in High-Temperature Reactors and Solid Oxide Fuel Cells

“…For the carbon deposition study, Ni was electrodeposited onto the Pt electrodes using a Watts bath consisting of a solution of 0.647 M H 3 BO 3 , 0.285 M NiSO 4 ·6H 2 O, and 0.047 M NiCl 2 ·6H 2 O. , Nitrogen was bubbled through the solution to rid the chamber of oxygen as well as being used during the plating experiments to rid the sample surface of H 2 bubbles formed. Nickel was used as the counter electrode together with a Hg/Hg 2 Cl 2 (SCE) reference electrode.…”

Application of a GaPO4 Crystal Microbalance for the Detection of Coke Formation in High-Temperature Reactors and Solid Oxide Fuel Cells

“…For the carbon deposition study, Ni was electrodeposited onto the Pt electrodes using a Watts bath consisting of a solution of 0.647 M H 3 BO 3 , 0.285 M NiSO 4 ·6H 2 O, and 0.047 M NiCl 2 ·6H 2 O. , Nitrogen was bubbled through the solution to rid the chamber of oxygen as well as being used during the plating experiments to rid the sample surface of H 2 bubbles formed. Nickel was used as the counter electrode together with a Hg/Hg 2 Cl 2 (SCE) reference electrode.…”

Application of a GaPO4 Crystal Microbalance for the Detection of Coke Formation in High-Temperature Reactors and Solid Oxide Fuel Cells

“…For the carbon deposition study, Ni was electrodeposited onto the Pt electrodes using a Watts bath consisting of a solution of 0.647 M H 3 BO 3 , 0.285 M NiSO 4 ·6H 2 O, and 0.047 M NiCl 2 ·6H 2 O. , Nitrogen was bubbled through the solution to rid the chamber of oxygen as well as being used during the plating experiments to rid the sample surface of H 2 bubbles formed. Nickel was used as the counter electrode together with a Hg/Hg 2 Cl 2 (SCE) reference electrode.…”