A comparative study of water-steam distillation with water-bubble distillation techniques to increase the quality of patchouli essential oil

Fitri, Noor; Yandi, Nefri; Hermawati, -; Julianto, Tatang Shabur

doi:10.1063/1.4978195

Cited by 5 publications

(4 citation statements)

References 7 publications

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“…There is also the development of other distillation methods such as the water-bubble distillation (WBD) method as in a study reported by Fitri [33], which compares the quality of patchouli oil extracted through the water-steam distillation (WSD) method. Yields produced by the WSD method are higher (5.90 %) than WBD (2.40 %).…”

Section: The Efficiency Of the Aceh Patchouli Oil Extraction Methodsmentioning

confidence: 99%

Mini-Review: Extraction of Patchouli Oil from Pogostemon cablin Benth. Leaves

et al. 2023

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Pogostemon cablin Benth. var ‘Sidikalang’ leaves are the main source of patchouli oil which is used in the cosmetics and perfume industry because of its better fixative nature and provides the foreign exchange of around 60 % of Indonesia’s essential oil export revenues and is the largest patchouli oil supplier in the world with a contribution of 90 %. But apparently, several studies found that patchouli oil also has pharmacological activity such as aromatherapy, anti-influenza, antioxidants, and anti-microbial. This proves that leaves patchouli oil can be used as alternative medicine. Patchouli oil is composed of 20 main constituents, but the most important role as a determinant of the quality of patchouli oil is sesquiterpene patchouli alcohol (PA). The right extraction method is the most important factor so that the quality of patchouli oil is well maintained during the extraction process. Some methods that have been used for patchouli oil extraction include soxhlet, hydrodistillation, microwave-assisted hydrodistillation, microwave–air hydrodistillation, and water–bubble distillation. Microwave-assisted hydrodistillation and water–bubble distillation methods are more efficient methods for patchouli oil extraction. The microwave-assisted hydrodistillation method produces a yield of 1.9437 to 2.7227 % with a PA content of 26.32 % within 120 min to 126 min, and the water–bubble distillation method produces a yield of 2.40 % with a PA content of 61.53 % within 360 min.

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Section: The Efficiency Of the Aceh Patchouli Oil Extraction Methodsmentioning

confidence: 99%

Mini-Review: Extraction of Patchouli Oil from Pogostemon cablin Benth. Leaves

et al. 2023

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“…To date, four variants of this method are known: hydrodistillation, direct steam stripping, indirect steam stripping, and a technique called distillation with water-bubble distillation (Table 2). One of the advantages of these methods is the use of water, considerably reducing the generation of harmful waste for the environment, and due to their design, they are easily scalable and do not require complex technologies (Aramrueang et al 2019;Azmir et al 2013;Fitri et al 2017).…”

Section: Steam Distillationmentioning

confidence: 99%

“…In the particular case of distillation by water-bubbling, it is a relatively new method whose first report dates from 2017; it has been observed that this is a non-exhaustive extraction method. It has been evaluated in the extraction of patchouli (Pogostemon cablin) essence, showing a higher proportion of patchoulol, compared to stripping with steam and water, which gives the extract a higher quality (Fitri et al 2017).…”

Section: Steam Distillationmentioning

confidence: 99%

Factors that influence the extraction methods of terpenes from natural sources

González-Hernández,

Valdez-Cruz,

Trujillo-Roldán

2024

Chem. Pap.

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Due to their various applications, terpenes and terpenoids are secondary metabolites of industrial interest. These compounds can be found in a wide variety of organisms from virtually all biological kingdoms. However, it has been identified that various factors in the production process, such as the place and time of harvest, pretreatments, extraction, and purification, generate differences in the profile of terpenes and terpenoids that can be obtained from organisms. The first factor that influences the extraction of compounds is drying since an inappropriate choice of the drying method can lead to the loss of the compounds of interest or the appearance of others that arise due to the decomposition of the original molecules. Similarly, Soxhlet extraction is the most used method in the recovery of terpenoids due to its high extraction efficiency. However, unconventional extraction methods have proven to be effective alternatives for terpenoid recovery, particularly the use of microwave and high-pressure extraction, as well as the use of unconventional solvents, achieving extraction efficiencies equal to or greater than Soxhlet in shorter times. This review will address the differences observed in the extraction of terpenoids and the main factors that cause them, as well as a comparison of the advantages and disadvantages of the various methodologies for drying, extraction, and separation of these compounds.

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“…Te samples (1% v/v in hexane) were injected into GC by split mode with a split ratio of 1/100. Patchoulol identifcation and other volatile compounds were based on comparing the mass spectra obtained in the gas chromatograph with those obtained from the GCMS library and literature [35][36][37][38].…”

Section: Patchouli Oil Component Identifcation a Gas Chromatography-m...mentioning

confidence: 99%

The Flow Rate of the Condenser Cooling Water in the Distillation Process Increases the Quality and Quantity of Patchouli Oil

Smith,

Assagaf,

Suwarda

et al. 2024

The Scientific World Journal

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Indonesia is an important essential oil-exporting country globally, where 40 types of essential oils have been traded on the international market and are products of Indonesia. However, the quality and quantity of patchouli oil produced in Indonesia are still low. Most essential oil processing units use simple or traditional technology and generally have limited production capacity. This study aimed to obtain the optimum water flow rate in a condenser system for patchouli oil production in Maluku, Indonesia. Patchouli oil extraction from fresh patchouli leaves and twigs was carried out by increasing the condenser water discharge rate. Patchouli oil extraction with a condenser cooling water discharge treatment of 1.74 L/min and drying time for 5 days produced the highest patchouli oil yield of 1.4%. The greater the condenser water discharge rate, the better the yield and accumulation of patchouli oil recovery obtained. In addition, based on the results of the analysis of the composition of patchouli oil compounds with GCMS, it can be seen that 13 compounds can be detected in patchouli oil. The three main components of patchouli oil in all condenser cooling water treatments were alpha-guaiene, delta-guaiene, and patchouli alcohol. Considering the results of all parameters mentioned above, the treatment of the condenser cooling water discharge of 1.74 L/min and drying time for 5 days increases the quality and quantity of patchouli oil.

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A comparative study of water-steam distillation with water-bubble distillation techniques to increase the quality of patchouli essential oil

Cited by 5 publications

References 7 publications

Mini-Review: Extraction of Patchouli Oil from Pogostemon cablin Benth. Leaves

Mini-Review: Extraction of Patchouli Oil from Pogostemon cablin Benth. Leaves

Factors that influence the extraction methods of terpenes from natural sources

The Flow Rate of the Condenser Cooling Water in the Distillation Process Increases the Quality and Quantity of Patchouli Oil

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