2022
DOI: 10.5155/eurjchem.13.1.63-68.2183
|View full text |Cite
|
Sign up to set email alerts
|

Abstract: Iron(II) and manganese(II) complexes of N'-(1-(pyridin-2-yl)ethylidene)nicotinohydrazide (LH) have been synthesized and characterized by elemental analysis, IR, and 1H NMR spectroscopy. The crystal structure of the ligand has been determined by single crystal X-ray diffraction and electronic spectroscopic techniques. Crystal data for LH, C13H12N4O: Orthorhombic, space group Pbcn (no. 60), a = 18.0824(3) Å, b = 7.86555(14) Å, c = 16.1614(3) Å, V = 2298.60(7) Å3, Z = 8, T = 103 K, μ(Mo Kα) = 0.093 mm-1, Dcalc = … Show more

Help me understand this report

Search citation statements

Order By: Relevance

Paper Sections

Select...
5

Citation Types

0
6
0

Year Published

2022
2022
2024
2024

Publication Types

Select...
4

Relationship

0
4

Authors

Journals

citations
Cited by 4 publications
(6 citation statements)
references
References 28 publications
0
6
0
Order By: Relevance
“…Yellow crystals suitable for single crystal X-ray diffraction studies were obtained from the ethanolic ltrate aer 30 days. 36 2.1.2 Synthesis of the metal complex. The Schiff base, L 1 , (0.26 g, 0.5 mmol) was added to Zn(CH 3 OO − ) 2 $2H 2 O (0.046 g, 0.25 mmol) in a 25 mL ethanolic solution.…”
Section: Methodsmentioning
confidence: 99%
See 4 more Smart Citations
“…Yellow crystals suitable for single crystal X-ray diffraction studies were obtained from the ethanolic ltrate aer 30 days. 36 2.1.2 Synthesis of the metal complex. The Schiff base, L 1 , (0.26 g, 0.5 mmol) was added to Zn(CH 3 OO − ) 2 $2H 2 O (0.046 g, 0.25 mmol) in a 25 mL ethanolic solution.…”
Section: Methodsmentioning
confidence: 99%
“…The pale-yellow solution obtained was allowed to cool overnight, the products removed by ltration; washed with ethanol and stored in a desiccator. 36 2.1.3 X-ray crystallography. Orange single crystals (platelike with 0.952 × 0.685 × 0.264 mm 3 for L 2 ) was served for analysis.…”
Section: Methodsmentioning
confidence: 99%
See 3 more Smart Citations