2005
DOI: 10.1590/s0101-20612005000200008
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Abstract: RESUMOA presença de hidrocarbonetos aromáticos polinucleares (HPAs) em aguardentes foi investigada por cromatografia líquida (CLAE) após sua prévia extração em fase sólida (SPE). A separação foi realizada em uma coluna , LCPAH-octadecil silano (25cm x 4,6mm x 5 m) com gradiente acetonitrila/água e a quantificação utilizando detector de fluorescência. Os HPAs (naftaleno; acenaftaleno; fluoreno; fenantreno; antraceno; fluoranteno; pireno; 1,2-benzo(e)pireno; criseno; benzo(e)pireno; 2,3-benzo(a)antraceno; 1,2-be… Show more

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Cited by 28 publications
(27 citation statements)
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“…In another work related to quantify PAH in cachaça, the authors had reported BaP recovery of 99.4% and CV of 4.2%. 16 GarciaFalcon and Simal-Gandara 20 had obtained BaP recovery result of 94% and CV of 9% for white rum and recovery result of 100% and CV of 9% for red wine.…”
Section: Resultsmentioning
confidence: 97%
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“…In another work related to quantify PAH in cachaça, the authors had reported BaP recovery of 99.4% and CV of 4.2%. 16 GarciaFalcon and Simal-Gandara 20 had obtained BaP recovery result of 94% and CV of 9% for white rum and recovery result of 100% and CV of 9% for red wine.…”
Section: Resultsmentioning
confidence: 97%
“…These results are considered satisfactory for BaP determination 24 and they are in accordance with values reported by others authors for BaP analysis in food and beverages. 8,10,[15][16][17][18]25 Extraction procedures were evaluated to maximize recovery and decrease both time and solvent consumption. Three different extraction procedures were tested, one using only SPE cartridge for extraction and clean-up steps, and two others, solvent partition to extraction and silica gel column to clean-up.…”
Section: Resultsmentioning
confidence: 99%
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