With the development of a digital technology of computer-assisted manufacturing (CAD/CAM) and new age materials, the use of new types of occlusal splint is to consider. The aim of the present study was to evaluate the surface roughness (Ra) and wear behavior of different CAD/CAM materials against enamel antagonist through a simulated chewing test. A total of 75 specimens made from ethylene vinyl acetate (EVA), polymethyl methacrylate (PMMA), polycarbonate (PC), polyetheretherketone (PEEK), and polyethyleneterephthalate (PETG) as a control were polished to evaluate the Ra before loading by optical profilometry and further analyzed by scanning electron microscopy (SEM). Specimens of each group were subjected to thermomechanical fatigue loading in a chewing simulator (60000 cycles at 49 N with 5-55 °C thermocycling). The wear volume loss and change in Ra of each specimen after the simulated chewing were analyzed. One-way ANOVA, paired samples t test, and Pearson correlation analysis were performed for statistical analyzes. The result showed that the volume loss and Ra varied among the materials tested. EVA exhibited the greatest amount of Ra and volume loss (p < 0.001), while PEEK had the lowest values for both (p < 0.001). In terms of volume loss, there was no significant difference between PC and PMMA (p > 0.05). SEM investigations revealed different wear behaviors, especially in EVA. As PEEK showed significantly more favorable results, PEEK splints should be considered as a new therapeutic option for occlusal splint.

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This study investigates the effects of process parameters on the quality of products fabricated by fused deposition modeling (FDM), such as surface roughness and tensile strength. Polylactic acid (PLA) samples were built on a FDM machine at various layer thicknesses, nozzle temperature and deposition head velocity. The effect of cooling the samples during the process was also considered. The experimental study was performed according to a mixed type Taguchi L16 orthogonal array. The effectiveness of each parameter was also discussed by an analysis of variance (ANOVA). The tensile strength results were compatible with the optical images of the fracture surfaces while the surface roughness results were compatible with the surface topography of the parts along the thickness. The two dominant quality characteristics were found to be layer thickness and deposition head velocity. Lower layer thickness values yielded higher tensile strength and lower surface roughness. Use of a cooling fan and nozzle temperature were found to be the least effective parameters. Finally, the results indicated that tensile strength and surface quality of the FDM samples improved about 25 %, and 12 %, respectively at optimal process conditions.

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This study investigates the influence of using multifunctional epoxy Joncryl ADR 4468 chain extender (CE) on the properties of various polylactide (PLA)/thermoplastic polyurethane (TPU) (75 wt/25 wt) blend systems. The blends were based on two different TPU grades with ether‐ and ester‐based soft segment as the dispersed phase (i.e., TPUether and TPUester) and an amorphous and a semicrystalline PLA grades as the matrix (i.e., aPLA and scPLA). PLA appeared to be more compatible with the TPUester, which caused the enhancement of the impact strength and strain at break values of the blends more remarkably. The dynamic rheological experiments also confirmed that the CE revealed a better reactivity with TPUester than TPUether. This further enhanced the interfacial compatibility between the PLA and TPUester and thereby dramatically improved the impact strength and ductility of the PLA/TPUester blends, specifically those with 0.5 wt% CE. Meanwhile, aPLA as the matrix reflected the TPUs toughening effect more efficiently than scPLA. This was due to the possible shrinkage caused by the crystallization of scPLA matrix, which could deteriorate the interfacial interactions between the phases in the corresponding blends.