The β-Mn structure (π-phase) is revealed on contact and free surfaces of Fe 63 Mo 37 melt-spinning ribbons. The full-profile analysis (Rietveld analysis) of diffraction patterns for a mixture of polycrystalline phases has identified, along with the metastable π phase, bcc solid solutions, µ and σ phases, and an intermediate bcc phase in the Fe-Mo phase diagram.
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