Marine and ice-core records show that the Earth has experienced a succession of glacials and interglacials during the Quaternary (last ~2.6 million years), although it is often difficult to correlate fragmentary terrestrial records with specific cycles. Aminostratigraphy is a method potentially able to link terrestrial sequences to the marine isotope stages (MIS) of the deep-sea record 1,2 . We have used new methods of extraction and analysis of amino acids, preserved within the calcitic opercula of the freshwater gastropod Bithynia, to provide the most comprehensive dataset for the British Pleistocene based on a single dating technique. A total of 470 opercula from 74 sites spanning the entire Quaternary are ranked in order of relative age based on the extent of protein degradation, using aspartic acid (Asx), glutamic acid (Glx), serine (Ser), alanine (Ala) and valine (Val). This new aminostratigraphy is consistent with the stratigraphical relations of stratotypes, sites with independent geochronology, biostratigraphy and terrace stratigraphy [3][4][5][6] . The method corroborates the existence of four interglacial stages between the Anglian (MIS 12) and the Holocene in the terrestrial succession. It establishes human occupation of Britain in most interglacial stages after MIS 15, but supports the notion of human absence during the Last Interglacial (MIS 5e) 7 . Suspicions that the treeless 'optimum of the Upton Warren interstadial' at Isleworth pre-dates MIS 3 are confirmed. This new aminostratigraphy provides a robust framework against which climatic, biostratigraphical and archaeological models can be tested.Despite the importance of the terrestrial record for climate models, the difficulties of assigning specific sedimentary sequences to individual climate cycles restricts the use of these data in climate modelling. The British Quaternary is exceptional for the number of who used the extent of racemization in the amino acid L-isoleucine (to its diastereomer D-alloisoleucine, yielding an A/I value) in non-marine mollusc shells to build an aminostratigraphy of terrestrial sequences that could be linked to the marine oxygen isotope stratigraphy. Following debate concerning certain correlations, we developed a revised method of extraction and analysis 9 . Shells of freshwater gastropods (Bithynia and Valvata) from many of the original sites 10 have been re-analysed, confirming much of the A/I stratigraphy. However, it emerged that within-site and within-stage variability increases in shells from older sites. This variability probably results from diagenetic alteration of the biomineral carbonate from aragonite to the more thermodynamically stable calcite 10,11 .Our new method has five significant revisions, three of which reduced within-site variability. First, inter-species variation was minimised by analysing only a single genus of freshwater gastropod (Bithynia). Second, variability in amino acid concentration and D/L values was significantly lowered when samples were crushed to ≤ 500 μm and exposed ...
The Middle to Later Stone Age transition in Africa has been debated as a significant shift in human technological, cultural, and cognitive evolution. However, the majority of research on this transition is currently focused on southern Africa due to a lack of long-term, stratified sites across much of the African continent. Here, we report a 78,000-year-long archeological record from Panga ya Saidi, a cave in the humid coastal forest of Kenya. Following a shift in toolkits ~67,000 years ago, novel symbolic and technological behaviors assemble in a non-unilinear manner. Against a backdrop of a persistent tropical forest-grassland ecotone, localized innovations better characterize the Late Pleistocene of this part of East Africa than alternative emphases on dramatic revolutions or migrations.
International audienceThe transition from the Terminal Pleistocene to the Early Holocene is poorly represented in the geological and archaeological records of northern Arabia, and the climatic conditions that prevailed in the region during that period are unclear. Here, we present a new record from the site of Al-Rabyah, in the Jubbah basin (southern Nefud desert, Saudi Arabia), where a sequence of fossiliferous lacustrine and palustrine deposits containing an archaeological assemblage is preserved. Sedimentological and palaeoenvironmental investigations, both at Al-Rabyah and elsewhere in the Jubbah area, indicate phases of humid conditions, during which shallow lakes developed in the basin, separated by drier periods. At Al-Rabyah, the end of a Terminal Pleistocene phase of lake expansion has been dated to ∼12.2 ka using optically stimulated luminescence (OSL), with a mid-Holocene humid phase dated to after ∼6.6 ka. Palaeoecological reconstructions based primarily on non-marine molluscs and ostracods from the younger lacustrine deposits indicate a relatively shallow body of freshwater surrounded by moist, well-vegetated environments. A lithic assemblage characterized by bladelets and geometric microliths was excavated from sediments attributed to a drier climatic phase dated to ∼10.1 ka. The lithic artefact types exhibit similarities to Epipalaeolithic industries of the Levant, and their occurrence well beyond the ‘core region’ of such assemblages (and at a significantly later date) has important implications for understanding interactions between Levantine and Arabian populations during the Terminal Pleistocene–Early Holocene. We suggest that the presence of foraging populations in the southern Nefud during periods of drier climate is due to the prolonged presence of a freshwater oasis in the Jubbah Basin during the Terminal Pleistocene–Early Holocene, which enabled them to subsist in the region when neighbouring areas of northern Arabia and the Levant were increasingly hostile
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