MgSOi), the solvent was removed under reduced pressure, and the residue was fractionally distilled to give benzaldehyde (2.10 g, 19.79 mmol, 79%), benzyl alcohol (2.25 g, 20.80 mmol, 83%), and unreacted dibenzyl ether (0.55 g, 2.77 mmol, 11%).Reaction of Dibenzyl Ether with Ethyl Azodicarboxylate.-A mixture of dibenzyl ether (1.14 g, 5.74 mmol) and 1 (1.00 g, 5.74 mmol) was heated at 140°for 30 min to give a colorless solid: ir (neat) 3280 (NH), 1740 cm'1 (C=0); nmr (CDClj) 7.36
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