We report the synthesis of a two-dimensional enamine-linked covalent organic framework (COF) using a rapid microwave-assisted solvothermal method in significantly less time and high yield under a relatively low temperature. This COF was found to have a high crystallinity, high stability, high BET surface area, and a high CO2 capacity and adsorption selectivity of CO2/N2.
A novel b-ketoenamine-linked conjugated microporous polymer (KECMP-1) was facilely synthesized with a high-throughput via Schiff base microwave-assisted condensation between 1,3,5-triformylphloroglucinol and m-phenylenediamine without a template or a metal catalyst. The resultant KECMP-1 shows an outstanding capacitance retaining ability (50% of the original 252 F g À1 at 1 A g À1 ) with the current density as high as 200 A g À1 , excellent cycling stability and long cycle life for energy storage.
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