The need to add value to cultivated and native plant products that have medicinal and nutritional properties is increasing due to the consumers demand. Nowadays, the bioactive compounds (phytochemicals) found in plants have many uses in the therapeutic, pharmaceutical, and food industries. Dried Roselle calyces (Hibiscus sabdariffa L.) are commercially available and appreciated to obtain concentrated extracts which might be used in the food and pharmaceutical industries. It has been shown that ingestion of infusions of Roselle may help to reduce chronic diseases such as diabetes mellitus, dyslipidemia, and hypertension. This could be due to the activity of some compounds, mainly flavonoids and anthocyanins, found as natural antioxidants in Roselle extracts. Numerous researchers have pointed out that Roselle and its extracts possess functional properties from where advances can be taken for developing new products with additional nutritious characteristics that may provide health benefits to consumers. Food products from Roselle are known as functional foods, which may provide health benefits to consumers because of its significant contribution of phytochemicals. In this sense, one of the main challenges that companies face todays is the development of new value-added products to meet the consumer's demands. This article presents a review of the most relevant aspects of Roselle as well as its health benefits and its application in the food and beverage areas.
SUMMARY Research has focused on the study and design of new products containing phytochemicals (polyphenolic acids, flavonoids and anthocyanins, among others) that contribute to a better life quality for consumers, as well as techniques to improve the extraction of these compounds. In this regard, extraction with supercritical fluids (usually CO 2 ) is a technology that has better advantages than organic solvents, since lower temperatures that are used do not damage the product, and is more effective at high pressures. Extracts from plant sources contain significant concentrations of flavonols, one of the main compounds being kaempferol. Research has proven the antioxidant, anticarcinogenic, antidiabetic, cardioprotective, neuroprotective and antimicrobial properties of kaempferol and its glycosides. This review aims to present the main functional properties and extraction with supercritical fluids of kaempferol and its glycosides, as well as the application of this technology in the food area.
This study compared the stability of extracts of calyces microencapsulated with different concentrations of mesquite gum during storage. Dry Roselle calyces were mixed with 50:50 (v/v) ethanol:water solution to obtain 18°Bx concentrate. This Roselle extract concentrate was mixed with purified mesquite gum (100:1-100:5 v/w). The Roselle extract concentrate-gum (RECG) was spray dried at inlet and outlet temperatures of 180 ± 2 and 104 ± 2.3 °C, respectively, at an air flow rate of 38 m/h. Encapsulated Roselle powders (ERP) were analyzed for moisture content, total monomeric anthocyanins (differential pH), phenolic compounds (Folin and Ciocalteu method), antioxidant capacity (ABTS), and color parameters ([Formula: see text], and [Formula: see text]) after 5 weeks and 1 year of storage. Sorption properties (isotherms) and micrographs of powders were also obtained. The average yield of RECG powders was 15.27 ± 0.81 g/100 mL. During storage, ERP showed average values of phenolic compounds, antioxidant capacity, and anthocyanins of 3.43 ± 0.25 g gallic acid equivalents/100 g, 9.34 ± 1.4 g Trolox equivalents/100 g, and 318.7 ± 20.6 mg cyanidin--glycoside/100 g, respectively. Color parameters remained constant along the storage time.
The effect of average particle size (APS), type of solvent, and extraction times (ET) on the physicochemical (moisture, pH, total soluble solids (TSS), titratable acidity, color, water activity (a w ), density), and phytochemical (total anthocyanins and phenols content)propertiesin Hibiscus sabdariffa (Roselle) calyces was analyzed. The phytochemical properties evaluation was performed using a factorial design 2×3×3: two APS (median diameters, d 50 , of 0.55 ± 0.016 (fine powder) and 0.97 ± 0.034 (ground powder) mm), three solvents (water, 2% citric acid, and 50% ethanol) and three ET (30, 45, and 60 min). All extractions were performed at 50 °C. The APS was determined by sieve analysis using Tyler sieves of different number of mesh. Regarding physicochemical properties, no significant differences (p > 0.05) were observed in moisture content, pH, and titratable acidity; however, the 0.55 mm fine powder (FP) of Hibiscus calyces had lower a w (0.37±0.01) and higher TSS (5.53±0.05%) than the 0.97 mm ground powder (GP). The extracts obtained fromGP showed a deeper red color than those of FP. The best combination of independent variables, in order to obtain the highest concentration of anthocyanins (451.4±28.1 mg/100 g d.s.) and total phenols (2016.2 ± 159.8 mg/100 g d.s.) were APS of 0.55 mm, 50% ethanol, and ETof 30 min.
Microencapsulation by spray drying is one of the most common methods used to obtain food material powders. In this study, different gums (maltodextrin [MD], gum arabic [GA], and mixtures of MD:GA [60:40] at various concentrations [0–10% w/w]) were used to microencapsulate Hibiscus sabdariffa (Roselle) extracts by spray drying. The yield, physicochemical properties, and antioxidant characteristics (total monomeric anthocyanins [TMAs], total phenolic compounds [TPCs], and antioxidant capacity [AC]) of the microencapsulated Roselle powders (RP) were evaluated. The highest RP yield (73.3 ± 3.3%) was obtained with the 3% MD:GA blend. The red color (a*) average for all powders (39.9 ± 2.0) decreased as the gum concentration increased. The 3% MD:GA RP showed the highest amount of TMAs (539.19 ± 13.27 mg cyaniding-3-glucoside equivalents/100 g) and TPCs (3,801.6 ± 125.9 mg of gallic acid equivalents/100 g of powder). The highest AC was observed with a 5% GA RP (1498.5 ± 44.0 mg of Trolox equivalents/100 g of powder).
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