M. Van Roelenbosch scite author profile

SummaryThis paper describes the results of a study on the deactivation of the surface of glass capillary columns by high temperature silylation (HTS).The different steps, leaching, washing, dehydration and HTS were optimized. A practical procedure yielding a high percentage of very good columns is given. The influence of leaching and HTS on the temperature stability and coating efficiency of capillary columns coated with OV-1 was studied. The inertness of the glass surface after HTS is demonstrated by several examples.

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Experiments with cold on-column injection

Sandra

Roelenbosch

Verzele

et al. 1983

Journal of Chromatography A

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M. Van Roelenbosch

In situ gummification of methylphenylsilicones in fused-silica capillary columns

Characterization, evaluation and in-situ cross-linking of new polar phases in capillary gas chromatography

Mixed phases of Superox 20M and OV-1 in fused silica and glass capillary gas chromatography

High temperature silylation of glass capillary columns

Experiments with cold on-column injection

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