A simple quasi-2D model for the temperature distribution in a graphite tube furnace is presented. The model is used to estimate the temperature gradients in the furnace at temperatures above which contact sensors can be used, and to assist in the redesign of the furnace heater element to improve the temperature gradients. The Thermogage graphite tube furnace is commonly used in many NMIs as a blackbody source for radiation thermometer calibration and as a spectral irradiance standard. Although the design is robust, easy to operate and can change temperature rapidly, it is limited by its effective emissivity of typically 99.5-99.8%. At NMIA, the temperature gradient along the tube is assessed using thermocouples up to about 1,500 • C, and the blackbody emissivity is calculated from this. However, at higher operating temperatures (up to 2,900 • C), it is impractical to measure the gradient, and we propose to numerically model the temperature distributions used to calculate emissivity. In another paper at this conference, the model is used to design an optimized heater tube with improved temperature gradients. In the model presented here, the 2-D temperature distribution is simplified to separate the axial and radial temperature distributions within the heater tube and the surrounding insulation. Literature data for the temperature dependence of the electrical and thermal conductivities of the graphite tube were coupled to models for the thermal conductivity of the felt insulation, particularly including the effects of allowing for a gas mixture in the insulation. Experimental measurements of the 2119 temperature profile up to 1,500 • C and radial heat fluxes up to 2,200 • C were compared to the theoretical predictions of the model and good agreement was obtained.
A key comparison between seven national metrology institutes in the area of low-pressure gas flow was organized by the Comité International des Poids et Mesures (CIPM) and the Working Group for Fluid Flow. A set of eight critical flow venturis with dedicated, redundant pressure and temperature sensors was used as the transfer standard at flows between 4.4 g/min and 260 g/min. Preliminary testing in the pilot lab determined temperature operating bounds and corresponding uncertainties. The transfer standard contributed a standard uncertainty of <0.026% to the comparison, primarily due to environmental temperature effects, the pressure sensors, and gas properties (the critical flow function and molecular mass of moist air). Redundant measurements by the transfer standard and the star pattern testing were valuable for maintaining low transfer standard uncertainty. The results supported equivalence between the labs with the largest difference between any two participants at any of the flows tested being 0.308%.Main text. To reach the main text of this paper, click on Final Report. Note that this text is that which appears in Appendix B of the BIPM key comparison database kcdb.bipm.org/.The final report has been peer-reviewed and approved for publication by the CCM, according to the provisions of the CIPM Mutual Recognition Arrangement (MRA).
The comparison CCM.FF-K6.2011 was organized for the purpose of determination of the degree of equivalence of the national standards for low-pressure gas flow measurement over the range (2 to 100) m3/h. A rotary gas meter was used as a transfer standard. The measurements were provided at prescribed reference conditions. Eleven laboratories from four RMOs participated in this key comparison—EURAMET: PTB, Germany; SMU, Slovakia; LNE-LADG, France; SIM: NIST, USA; CENAM, Mexico; APMP: NMIJ AIST Japan; KRISS, Korea; NMI, Australia; NIM, China; CMS, Chinese Taipei; COOMET: GP GP Ivano-Frankivs'kstandart-metrologia, Ukraine and all participants reported independent traceability chains to the SI. All results were used in the determination of the key comparison reference value (KCRV) and the uncertainty of the KCRV. The reference value was determined at each flow separately following procedure A presented by M G Cox. The degree of equivalence with the KCRV was also calculated for each flow and laboratory. All reported results were consistent with the KCRV. This KCRV can now be used in the further regional comparisons.Main text. To reach the main text of this paper, click on Final Report. Note that this text is that which appears in Appendix B of the BIPM key comparison database kcdb.bipm.org/.The final report has been peer-reviewed and approved for publication by the CCM, according to the provisions of the CIPM Mutual Recognition Arrangement (CIPM MRA).
Design modifications are presented for a 289-mm long, 25.4-mm inner diameter blackbody heater element of a 48 kW Thermogage blackbody furnace, based on (i) cutting a small "heater zone" into the ends of the tube and (ii) using a mixture of He and Ar or N 2 to "tune" the heat losses and, hence, gradients in the furnace. A simple numerical model for the heater tube is used to model and optimize these design changes, and experimental measurements of the modified temperature profile are presented. The convenience of the Thermogage graphite-tube furnace, commonly used in many NMIs as a blackbody source for radiation-thermometer calibration and as a spectral irradiance standard, is limited by its effective emissivity, typically between 99.5% and 99.9%. The design simplicity of the furnace is that the blackbody cavity, heater, and electrical and mechanical connections are achieved through a single piece of machined graphite. As the heater also performs a mechanical function, the required material thickness leads to significant axial heat flux and resulting temperature gradients. For operation at a single temperature, changes to the tube profile could be used to optimize the gradient. However, it is desired to use the furnace over a wide temperature range (1,000-2,900 • C), and the temperature-dependence of the electrical conductivity and thermal conductivity, and that of the insulation, makes this approach much more complex; for example, insulation losses are proportional to T 4 , whereas conduction losses are proportional to T . In the results presented here, a slightly thinner graphite region near each end of the tube was used to "inject heat" to compensate for the axial conduction losses, and the depth, width, and position of this region was 123 Int J Thermophys (2008) 29:386-394 387 adjusted to achieve a compromise in performance over a wide temperature range. To assist with this optimization, the insulation purging gas was changed from N 2 to He at the lower temperatures to change the thermal conductivity of the felt insulation, and the effectiveness of this approach has been experimentally confirmed.
This APMP key comparison of humidity measurements using a dew point meter as a transfer standard was carried out among eight national metrology institutes from February 1999 to January 2001. The NMC/SPRING, Singapore was the pilot laboratory and a chilled mirror dew point meter offered by NMIJ was used as a transfer standard. The transfer standard was calibrated by each participating institute against local humidity standards in terms of frost and dew point temperature. Each institute selected its frost/dew point temperature calibration points within the range from -70 °C to 20 °C frost/dew point with 5 °C step. The majority of participating institutes measured from -60 °C to 20 °C frost/dew point and a simple mean evaluation was performed in this range. The differences between the institute values and the simple means for all participating institutes are within two standard deviations from the mean values. Bilateral equivalence was analysed in terms of pair difference and single parameter Quantified Demonstrated Equivalence. The results are presented in the report.
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