Clinical procedures when shear forces are applied to brackets suggest adhesion forces between 2.8 and 10.0 MPa as appropriate. In this study dental enamel was evaluated by scanning electron microscopy (SEM) before and after removing the brackets. Thirty bicuspids (previous prophylaxis) with metallic brackets (Roth Inovation 0.022 GAC), Transbond Plus SEP 3M Unitek adhesive and Transbond XT 3M resin were used. The samples were preserved to 37°C during 24 hr and submited to tangential forces with the Instron Universal machine 1.0 mm/min speed load strength resistance debonding. Also the Adhesive Remanent Index (ARI) test was made, evaluating the bracket base and the bicuspid surface. All the bracket SEM images were processed with AutoCAD to determine the enamel detached area. The average value was 6.86 MPa (SD ± 3.2 MPa). ARI value 1= 63.3%, value 2= 20%, value 3= 13.3% and 33% presented value 0. All those samples with dental enamel loss, presented different situations as fractures, ledges, horizontal, and vertical loss in some cases, and some scratch lines. There is no association between the debonding resistance and enamel presence. Less than half of the remanent adhesive on the dental enamel was present in most of the samples when the ARI test was applied. When the resin area increases, the debonding resistance also increases, and when the enamel loss increases, the resin free metallic area of the bracket base decreases in the debonding.
The aim of the present study is to obtain structural and chemical information about nucleation and growth of dental enamel as a function of location in secretory mouse foetus enamel. Then enamel tissues were obtained from 19-days-mouse foetus. TEM images show that enamel crystallites had the well-documented thin ribbons, or needles. They were found in the outermost zone in the vicinity of ameloblasts. Chemical analysis by EDS showed that, besides the elements of hydroxyapatite, Na, Cl, Al and Mg are presents from the beginning of enamel mineralization. All of these elements will play an important role on the physics and chemical properties in mature enamel.
CRYSTALLOGRAPHY IN MATERIAL SCIENCE C390 orientation of the grains in the marginal and central zones of the walls or the lack of the preferential orientations, associated with some obvious directional changes in the very limited spaces. emphasizing in such way different techniques of moulding-fashioning of the ceramic paste. No engobe has been identified. Though, they have been found in the same area and they are considered contemporary, the mineralogical aspects emphasize (i) different historical periods, (ii) the same period, but some changes in the processing of ceramic material could taken place, or (iii) different geographical areas, for their origin.
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