The rolling operation consists of deforming the material by passing it between two rolls whose spacing is smaller than the initial thickness of the sample, the reduction in thickness is obtained discontinuously by successive passes in the rolling mill whose spacing between the cylinders gradually decreases. This operation can influence on the mechanical and microstructural properties of the deformed materials The effect of cold rolled on microstructural evolution and precipitation sequence in Al-Mg-Si alloy has been investigated by using optical microscopy and Differential Scanning Calorimetry (DSC) in this study . The results revealed that the distribution of the grains are elongated along the rolling direction. We also noted that i nsoluble coarse particles that originated during the manufacturing process of the alloy have become visible after the rolling processes . The dislocations generated by the plastic deformation during cooled rolling constitute preferential sites for the germination and the growth of the phases, which accelerates the kinetics of the precipitation.
Rolling is a very common technique for shaping sheet metal. It aims to reduce the thickness of a metal sample to adapt it to the usual conditions of use in the industry. Nevertheless, this technique is not without modifying the mechanical and microstructural properties of the materials that can influence the mechanical strength of shaped parts. The purpose of the present investigation is to study the changes in microstructures and micro-hardness of Al-Mg-Si alloy with different rolling reduction in thickness and following artificial aging treatments at 175° C . We notice that the micro-hardness increases with the increasing of the deformation level . Reduction in thickness shows a change in microstructure and texture. Characterization methods used in this work is: Optical Microscopy (OM) and, Vickers microhardness.
The scope of this work is to investigate the precipitation of two Al-Mg-Si alloys with and without Cu and excess Si by using the differential scanning calorimetry (DSC), transmission electron microscopic (TEM), Vickers hardness measurement and X-ray diffraction. The analysis of the DSC curves found that the excess Si accelerate the precipitation and the alloy contain the excess Si and small addition of copper has higher aging-hardness than that of free alloy (without excess Si and Cu) at the same heat treatment condition. The sufficient holding time for the precipitation of the β'' phase was estimated to be 6 hours for the alloy aged at 100°C and 10 hours for the alloy aged at 180°C. The low Copper containing Al-Mg-Si alloy gives rise to the forming a finer distribution of β (Mg 2 Si) precipitates which increases the hardness of the alloy. In order to know more about the precipitation reactions, concern the peaks on the DSC curve transmission electron microscopy observation were made on samples annealed at temperatures (250°C, 290°C and 400°C) just above the corresponding peaks of the three phases β'', β' and β respectively.
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