The concentration and the chemical composition of the essential oils obtained from different samples of Cymbopogon citratus were evaluated. Among the 12 samples investigated (11 dried leaf samples and fresh plant leaves), seven presented essential oil concentrations within the threshold established by the Brazilian legislation. The moisture content was also determined and the majority of the samples presented humidity contents near 12%. The GC and GC/MS analyses of the essential oils led to identification of 22 compounds, with neral and geranial as the two major components. The total percentage of these two compounds varied within the investigated sample oils from 40.7% to 75.4%. In addition, a considerable variation in the chemical composition of the analyzed samples was observed. The process of grinding the leaves significantly decreased (by up to 68%) the essential oil content, as well as the percentage of myrcene in the oils.
As características da secagem de folhas de Cymbopogon citratus (D.C.) Stapf em camada delgada, foram estudadas para a faixa de temperatura de 30-60 ºC, utilizando-se modelos semi-teóricos e empíricos. O modelo de Midilli foi o que melhor descreveu as curvas de secagem. Os valores da difusividade efetiva variaram de 4 x 10-12a 3,9 x 10-11 m-2 s-1 para a faixa de temperatura avaliada. Os valores obtidos da difusividade efetiva mostraram uma dependência de Arrhenius. O valor da energia de ativação encontrado foi de 63,47 kJ mol- 1.
This study aims to evaluate the quality of lemongrass plants after drying at different speeds (1.0, 1.5, 2.0 m s À1 ), temperatures (40, 50, 60, and 70 C), and drying air control systems (manual and automatic) using electrical conductivity as a parameter for evaluation. Firstly, we evaluated the time necessary for imbibitions of material in deionized water after drying for different air speeds and control systems. Secondly, the effect of temperature in fresh and dry plants was evaluated, comparing them with contents of essential oils and the quantity of ions leached by the electrical conductivity test. According to the results, the value of liquid diffusion increased with the increase of drying air temperature, and the value of activation energy was 62.84 kJ mol À1 . The quality of lemongrass plants evaluated by the electrical conductivity test was inversely proportional to the increase in drying air temperature, and the levels of essential oils were higher in dry plants with lower drying air temperatures. The adaptation of the electrical conductivity methodology to lemongrass plants was effective. A period of 33 h of imbibitions of the material in deionized water was necessary to obtain consistent results from leaching of potassium ions. The electrical conductivity can be used as a quality parameter for drying of medicinal plants.
Los objetivos del trabajo fueran estudiar la cinética del secado de tomillo con posterior ajuste de diferentes modelos matemáticos a los datos experimentales y determinar los valores de la difusividad efectiva y energía de activación. Para el desarrollo del experimento de secado fueran utilizadas las temperaturas 30, 40, 50, 60 y 70 oC. El diseño experimental fue de bloques completamente aleatorizados, con tres repeticiones. Para el ajuste de los modelos matemáticos a los datos experimentales fue realizado el análisis de regresión no lineal, por el método Simplex-Quasi-Newton. Los resultados mostraron que el modelo matemático de Page obtuve un mejor ajuste a los datos experimentales, los valores de los coeficientes de difusividad efectiva variaron entre 3,69 x 10-12 e 1,19 x 10-10 m² s-1 y el valor de la energía de activación fue de 77,16 kJ mol-1.
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