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A methodological analysis is made in the rational synthesis of the Bi2O3/Ag2O nanostructure with significant application, possessing substantial electron-hole recombination acting as solar catalysts through powerful and modest hydrothermal technique. The composite Bi2O3/Ag2O is intermediary for single step Methyl Red (MR) dye photocatalytic degradation. Under the impact of solar irradiation heavy metals like, Lead (Pb) are also removed by the synthesized material surface influence of sunlight. Anti-cancer activity upon Colon cancer cells (HCT116) is achieved with excellent cell viability and IC50 value. The research work or the present study found an excellent and efficient design of photocatalyst as an eco-friendly and biomedical approach.