In this work, an energy-efficient extractive dividingwall column process with heat integration (E-DWC-HI) is proposed for the first time to separate the dichloromethane (DCM)−methanol (MeOH) azeotrope, which is a widely existing waste effluent in the pharmaceutical industry. The result of economic evaluation shows that the E-DWC-HI process is a preferred choice for the separation of DCM−MeOH mixture. Designing a robust control strategy is essential for the E-DWC-HI process. Thus, four control structures are proposed and tested under the disturbances of ±20% feed flow rate and ±5% feed composition. The basic control structure (CS1) and the double temperature difference control structure (CS2) both have a fixed vapor split. The dynamic response shows that the required purity cannot be met due to the loss of an important control degree of freedom. In CS3, variable vapor split is carried out by adjusting the pressures on the two sides of the dividing wall, and all product purities are held close to their set points except for MeOH product purity with an obvious offset. The dynamic performance of CS4 has been significantly improved by integrating pressure swing and pressure compensation. The offset of MeOH product purity is significantly reduced from 2.05 to 0.03%.
Designed new table for large floor boring and milling machine, used ANSYS to optimize the structure of the table as a whole. According to the contours of removable material the materials which can be removed, obtained the inner ribs layout of table and the sand holes location of rib plate. Dynamic optimization variables on basic ribs cell, studied the effect of steel lattice structure parameters influenced on the natural frequency of the lattices and the related parameter of lattices influenced on whole table, to get the ideal rib lattice structure after optimizing again. Optimized bench can reduce quality, increase rigidity and dynamic performance.
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