Aiming to reduce aircraft weight, aeronautic industry seeks alternative materials and processes used to join its different structural parts. An option to traditional methods are high performance adhesive joints, which reduce weight, number of parts and component final cost, also resulting in higher strength structures. Although, the lack of experimental data to provide a detailed structural characterization of these joining techniques had limited their commercial application. The proposal of this work is to investigate the Mode I interlaminar fracture toughness under quasi-static loading using DCB specimens of carbon composite joints made by co-bonding and secondary bonding techniques, the latter giving more reliable results. For a better understanding on the failure in the systems, DSC and microscopy techniques were applied, from which three stages of delamination process during testing were observed: 1 st Stage) Cohesive failure represented by an unstable crack propagation from a high energy level; 2 nd Stage) transition from cohesive to adhesive and final intralaminar failure mode with lower energy levels than Stage 1; and 3 rd Stage) completely stable propagation at low energy levels (delamination migrates from intralaminar to interlaminar, entirely in the substrate).

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Adhesive joints are being more extensively applied in the aeronautical industry, allowing for better integration between the structural parts and overall lower weight if compared with joints made with fasteners and rivets. However, a further evaluation of these new technologies is needed, once their critical fracture toughness under different environmental conditions is still unknown and this value is essential for design and certification of aircraft manufactured with these materials. Thus, this work focuses on the mode II fracture toughness characterization of carbon fiber composite laminates joined by co‐bonded (CB) and secondarily bonded (SB) techniques, using EA 9695 epoxy adhesive aged at different environmental conditions (room temperature ambient—RTA and elevated temperature wet—ETW). Dynamic mechanical analysis (DMA) was used to understand the effect of moisture absorption on the glass transition of materials and on the decreasing of Mode II fracture toughness after aging. The DMA results showed a reduction of 11% in Tg values for the GIIc values of ETW samples in comparison with specimens tested at RTA condition. Reductions about 92 and 94% in Mode II fracture toughnesses were obtained for CB and SB aged specimens, respectively when compared with the toughness values obtained for specimens tested at RTA. Further inspection of the fracture surfaces using scanning electron microscope proved that light fiber‐tear fracture occurred at both RTA and ETW conditions for CB joints, while fracture was mainly light‐fiber‐tear at RTA condition, becoming mostly cohesive after aging for SB joints. POLYM. COMPOS., 40:3220–3232, 2019. © 2018 Society of Plastics Engineers

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