Glyphosate detection and quantification is still a challenge. After an extensive review of the literature, we observed that Fourier transform infrared spectroscopy (FTIR) had practically not yet been used for detection or quantification. The interaction between zinc oxide (ZnO), silver oxide (Ag2O), and Ag-doped ZnO nanocrystals (NCs), as well as that between nanocomposite (Ag-doped ZnO/AgO) and glyphosate was analyzed with FTIR to determine whether nanomaterials could be used as signal enhancers for glyphosates. The results were further supported with the use of atomic force microscopy (AFM) imaging. The glyphosate commercial solutions were intensified 10,000 times when incorporated the ZnO NCs. However, strong chemical interactions between Ag and glyphosate may suppress signaling, making FTIR identification difficult. In short, we have shown for the first time that ZnO NCs are exciting tools with the potential to be used as signal amplifiers of glyphosate, the use of which may be explored in terms of the detection of other molecules based on nanocrystal affinity.
Glyphosate [(N-phosphonomethyl) Glycine], one of the most worldwide commercialized herbicides, has provoked many debates about its carcinogenic effects. Here, a smartphone-based surface plasmon resonance (SPR) sensor is proposed for glyphosate detection using different pH and concentrations. CuO nanoparticles have been added to glyphosate samples, diluted in ultra-pure water solutions, to enhance its detection. An increase of sensitivity was observed in acidic solutions reaching a dilution of 10 −8 (v/v), which is equivalent to 5 • 10 −7 ppm. This novel smartphonebased SPR device for glyphosate detection besides presenting very high sensitivity, it has also favorable features such as easy handling, portability, and real-time analysis.
<htm>Estratégia de maximização de sucesso de perseguição e fuga nos contextos de caça entre golfinhos <i>Sotalia guianensis </i>(Van Bénedén, 1864) e peixes no povoado de Pipa, RN </htm>
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