Simplified restorative materials may be a logical next step for dental manufacturers. Objective: The aim of this study was to evaluate the shear bond strength of a self-adhering flowable composite to four substrates used in indirect technique. Material and methods: Twenty-four samples (5 mm wide, 15 mm length and 2 mm thick / six blocks each substrate) were prepared in the dental prosthetic laboratory. The following materials were used: ceromer (SR Adoro/AD, Ivoclar Vivadent), leucite ceramic (IPS Empress Esthetic/EE, Ivoclar Vivadent), zirconia ceramic (ZirCAD/ZI, Ivoclar Vivadent); metal ceramic alloy (Fit Cast SB/ME, Talladium do Brasil). Samples of each substrate were divided into two groups (n = 3). Two flowable composites (Control/FF – Filtek Z350 XT Flow/3M ESPE, and the self-adhering/DF – Dyad Flow/Kerr) were bonded to the four substrates. Four Tygon tubings were positioned over each sample, which were filled in with the composites FF and DF, and visible light-cured for 20 s. The tubings were removed to expose the specimens (12 per group) in format of cylinders and samples were stored in distilled water at 37±2°C for one week. After this period, each sample was attached to testing machine and the specimens were submitted to the shear bond strength test at speed of 1.0 mm/min, until failure. The results were analyzed by two-way ANOVA and Tukey test (p < 0.05). Results: The means (SD) were (in MPa): AD + FF = 34.4 ± 4.9; AD + DF = 28.2 ± 4.2; EE + FF = 29.7 ± 5.8; EE + DF = 32.3 ± 6.9; ZI + FF = 23.2 ± 5.4; ZI + DF = 8.5 ± 1.5; ME + FF = 28.9 ± 4.2; ME + DF = 31.7 ± 4.5. Conclusion: The efficacy of flowable composites is material-dependent. The self-adhering composite provided lower bond strength only to zirconia ceramic. Comparing with the control group, Dyad Flow showed lower bond strength to the ceromer and zirconia ceramic.
Objective: The aim of this study was to compare the shear bond strength (SBS) of two resin cements bonded to four leucite-reinforced ceramics after one week and one year of aging. Material and methods: Forty ceramic blocks (4 mm wide, 14 mm length, and 2 mm thick) were used (1 week) and reused at the back side (1 year). The blocks were abraded with aluminum oxide (90 µm) and randomly divided into eight groups for each time. Two dual resin cements (RelyX ARC and RelyX U200 self-adhesive, 3M ESPE) were bonded to ceramics Creapress (CRE -Creation / Klema), Finesse All-Ceramic (FIN -Dentsply / Ceramco), IPS Empress Esthetic (IEE -Ivoclar Vivadent) and Vita PM9 (PM9-Vita). For each resin, time, and ceramic block, after applications of the 10% hydrofluoric acid (for 1 min) and silane, 3 Tygon cut tubes were positioned over each block and filled in with the resin cements (light-cured for 40 s). The tubing molds were removed to expose the bond specimens as cylinders (area=0.38 mm 2 ) stored in relative humidity at 24±2°C for one week and at 37±2°C for one year. All bonds were tested in an Instron in shear (applied of the base cylinder with a thin wire -0.25 mm) at speed of 0.5 mm/min, until failure. Results: The Garcia et al. -Bond strength of resin cements to leucite-reinforced ceramics: part 2 -after one-year aging in water results were analyzed by ANOVA (resin cements, ceramic systems, and time) and Tukey test (p<0.05) for rank ordering of SBS. The FIN and IEE ceramics did not show significant SBS decreasing on aging with U200. The mean SBS decreasing for all the ceramics was 36% with ARC and 14% with U200 cement. Conclusion: The SBS of ARC cement were significantly lower for all ceramics with aging than that of U200 cement. The SBS of ARC cement was also weakened by aging. FIN ceramic + U200 cement proved to be the most stable and strongest bond strength, and PM9+ARC cement proved to be the weakest bond strength with low stability.
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