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UDC 621.762.5:666.3/7Powder mixtures based on titanium and its dihydrides are sintered by electric discharge in a certain current mode to produce TiN + TiB 2 composites. It is established that the use of tetragonal titanium hydride as the starting material results in the complete synthesis leading to a TiN + TiB 2 composite. The higher shrinkage rate results from the higher purity of titanium dihydride, which, in its turn, increases the partial pressure of hydrogen in the reaction area and the reaction rate. Tetragonal titanium hydride is more preferable than cubic hydride and metal titanium. The microstructure of alloys resulting from the sintering of hydride-based mixtures is more homogenous: it includes equiaxial grains with the mean size of about 1 µm.