Novel special optical fibers nowadays can take advantage of several new preform production techniques. During the last years we have devoted our attention to the granulated silica method. It is one of the variants of the powder-in-tube technique and potentially offers a high degree of freedom regarding the usable dopants, the maximum possible dopant concentration, the homogeneity of the dopants, the geometry and minimal refractive index contrast. We developed and refined an approach for the production of doped granulated silica material based on the sol-gel process.Here, we present material analysis results of an ytterbium (Yb) doped, aluminum (Al) and phosphorous (P) co-doped glass on the basis of our sol-gel glass based granulated silica method as well as first measurements of two LMA fibers obtained from this material. For the material analysis we used advanced analysis techniques, such as HAADF-STEM and STEM-EDX spectroscopy to determine the composition of the material and the distribution of the dopants and the codopants. The chemical mapping of the STEM-EDX shows an extremely homogeneous distribution of the dopants and co-dopants in nano-scale. Based on self-made LMA fibers, we measured the refractive index contrast of the sol-gelbased granulated silica derived core compared to the pure silica cladding. In addition we quantified optical characteristics such as the emission and absorption spectrum. The measured upper state lifetime of the optical active dopant ytterbium was 0.99ms, which in turn confirms the homogeneous distribution of the Yb atoms. The propagation losses were determined to be 0.2dB/m at 633nm and 0.02414dB/m at1550nm.
Fabrication of Ytterbium--doped active fibers with different designs, compositions and high Yb concentration has attracted an intense interest. For making highly Yb--doped fibers, co--dopants like phosphorous (P) and aluminum (Al) are also employed in order to modify refractive index and increase Yb solubility, avoiding clusters and phase segregations. Indeed, Yb--clustering results in quenching effects and increased propagation losses due to energy transfer between clustered ions. Therefore, the chemical composition and phase homogeneity of the fiber core have key influences on the performance of an active fiber. However, conventional fabrication techniques such as MCVD (modified chemical vapor deposition) and OVD (outside vapor deposition) are approaching the limit.In this contribution, we have developed an approach for fabrication of such active fibres based on granulated silica derived from the sol--gel process. The advantage of this method is the fabrication of active fibers with high dopant contents and homogeneity. Here, using high angle annular dark--field scanning transmission electron microscopy (HAADF--STEM) in atomic scale, we report the direct, nano--scale and atomic--resolution observation of individual Yb dopant and co--dopant (i.e. Al, P) atoms for different fabricated fibers. The chemical mapping from STEM--EDX shows an extremely homogeneous distribution of the dopants and co--dopants in nano--scale for our fabrication protocol. However in atomic resolution, we also identified the possible Yb clusters in the range of 10 atoms within the core structure. The size, structure, and distribution of these clusters are determined with an Yb--atom detection efficiency of almost 100% by STEM.
The refractive index distribution in the core-cladding region of an optical fiber plays an important role in determining the transmission and dispersion properties of the waveguide. The refracted near-field technique (RNF) is among the most widespread techniques used for measuring the refractive index profile of optical fibers and is based on illuminating the end-facet of a fiber with a focused beam whose vertex angle greatly exceeds the acceptance angle of the fiber, which is immersed in an index matching liquid. What one observes are then the refracted unguided rays rather than the guided rays. Nevertheless, the standard refracted near-field technique cannot be applied to a wide range of optical fibers e.g. if their shapes are not axially symmetric. In this work we demonstrate a modified method which allows 2-D imaging of the refractive index profile and thereby overcoming the axial symmetric limitation of the standard RNF. The new system is operating at 630 nm and based on the same principle of the RNF, but the optical path is reversed so that the light at the fiber end-facet is collected by an objective lens and detected by a CCD camera. The method does not require scanning over the fiber end-facet. Thus the system is faster and less sensitive to vibrations and external conditions compared to the standard RNF, furthermore it allows averaging to improve the signal to noise ratio. The spatial resolution of the system is determined by the numerical aperture of the objective and by the resolution of the CCD camera. To calibrate the setup, a reference multi-step index fiber provided by National Physical Laboratory was used.
The refractive index distribution in the core-cladding region of an optical fiber plays an important role in determining the transmission and dispersion properties of the waveguide. The refracted near-field technique (RNF) is among the most widespread techniques used for measuring the refractive index profile of optical fibers and is based on illuminating the end-facet of a fiber with a focused beam whose vertex angle greatly exceeds the acceptance angle of the fiber, which is immersed in an index matching liquid. What one observes are then the refracted unguided rays rather than the guided rays. Nevertheless, the standard refracted near-field technique cannot be applied to a wide range of optical fibers e.g. if their shapes are not axially symmetric. In this work we demonstrate a modified method which allows 2-D imaging of the refractive index profile and thereby overcoming the axial symmetric limitation of the standard RNF. The new system is operating at 630 nm and based on the same principle of the RNF, but the optical path is reversed so that the light at the fiber end-facet is collected by an objective lens and detected by a CCD camera. The method does not require scanning over the fiber end-facet. Thus the system is faster and less sensitive to vibrations and external conditions compared to the standard RNF, furthermore it allows averaging to improve the signal to noise ratio. The spatial resolution of the system is determined by the numerical aperture of the objective and by the resolution of the CCD camera. To calibrate the setup, a reference multi-step index fiber provided by National Physical Laboratory was used.
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